dimethyl N-p-methoxybenzylidene-2-phenylglutamate

Base Information

• Chemical Name: dimethyl N-p-methoxybenzylidene-2-phenylglutamate
• CAS No.: 75984-48-4
• Molecular Formula: C₂₁H₂₃NO₅
• Molecular Weight: 369.417

Synonyms:dimethyl N-p-methoxybenzylidene-2-phenylglutamate

Chemical Property of dimethyl N-p-methoxybenzylidene-2-phenylglutamate

Chemical Property:

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Technology Process of dimethyl N-p-methoxybenzylidene-2-phenylglutamate

There total 1 articles about dimethyl N-p-methoxybenzylidene-2-phenylglutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

methyl N-4'-methoxybenzylidenephenylglycinate (63430-99-9,88967-39-9,120328-94-1,67628-17-5) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → dimethyl N-p-methoxybenzylidene-2-phenylglutamate (75984-48-4)

Guidance literature:

benzyltrismethylammonium methoxide; In benzene; for 24h; Ambient temperature;

DOI:10.1016/S0040-4020(01)86043-9

Reference yield: 59.0%

dimethyl N-p-methoxybenzylidene-2-phenylglutamate (75984-48-4) → dimethyl c-5-p-methoxyphenyl-2-phenyl-r-2,t-4-pyrrolidinedicarboxylate (75516-90-4,75516-94-8,75984-54-2,75984-59-7,119993-38-3,119993-39-4) + dimethyl t-5-p-methoxyphenyl-2-phenyl-r-2,c-4-pyrrolidinedicarboxylate (75516-90-4,75516-94-8,75984-54-2,75984-59-7,119993-38-3,119993-39-4)

Guidance literature:

benzyltrismethylammonium methoxide; In benzene; at 80 ℃; for 5h;

DOI:10.1016/S0040-4020(01)86043-9

upstream raw materials:

methyl N-4'-methoxybenzylidenephenylglycinate

acrylic acid methyl ester

Downstream raw materials:

dimethyl c-5-p-methoxyphenyl-2-phenyl-r-2,t-4-pyrrolidinedicarboxylate

dimethyl t-5-p-methoxyphenyl-2-phenyl-r-2,c-4-pyrrolidinedicarboxylate

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