N-(3-(3,5,7,9,11,13,15-heptaisobutyl)pentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propyl-4-(6-(4-(4-methoxy)phenylazo)phenoxy)hexyloxybenzamide

Base Information

Chemical Name:N-(3-(3,5,7,9,11,13,15-heptaisobutyl)pentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propyl-4-(6-(4-(4-methoxy)phenylazo)phenoxy)hexyloxybenzamide
CAS No.:1346774-35-3
Molecular Formula:C₅₇H₉₇N₃O₁₆Si₈
Molecular Weight:1305.09
Hs Code.:

N-(3-(3,5,7,9,11,13,15-heptaisobutyl)pentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propyl-4-(6-(4-(4-methoxy)phenylazo)phenoxy)hexyloxybenzamide

Synonyms:N-(3-(3,5,7,9,11,13,15-heptaisobutyl)pentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propyl-4-(6-(4-(4-methoxy)phenylazo)phenoxy)hexyloxybenzamide

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Chemical Property of N-(3-(3,5,7,9,11,13,15-heptaisobutyl)pentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propyl-4-(6-(4-(4-methoxy)phenylazo)phenoxy)hexyloxybenzamide

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Technology Process of N-(3-(3,5,7,9,11,13,15-heptaisobutyl)pentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propyl-4-(6-(4-(4-methoxy)phenylazo)phenoxy)hexyloxybenzamide

There total 8 articles about N-(3-(3,5,7,9,11,13,15-heptaisobutyl)pentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propyl-4-(6-(4-(4-methoxy)phenylazo)phenoxy)hexyloxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: C₂₆H₂₇ClN₂O₄

: 444315-15-5
3-(3,5,7,9,11,13,15-heptaisobutylpentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propylamine

: 1346774-35-3
N-(3-(3,5,7,9,11,13,15-heptaisobutyl)pentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propyl-4-(6-(4-(4-methoxy)phenylazo)phenoxy)hexyloxybenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 6h; Reflux;
DOI:10.1039/c1nj20577c

Reference yield:

: 307531-92-6
1,3,5,7,9,11,14-heptaisobutyltricyclo[7.3.3.15,11]heptasiloxane-endo-3,7,14-triol

: 1346774-35-3
N-(3-(3,5,7,9,11,13,15-heptaisobutyl)pentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propyl-4-(6-(4-(4-methoxy)phenylazo)phenoxy)hexyloxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetraethylammonium hydroxide / methanol; ethanol / 36 h / 20 °C

2: triethylamine / dichloromethane / 6 h / 0 °C / Reflux

With tetraethylammonium hydroxide; triethylamine; In methanol; ethanol; dichloromethane;
DOI:10.1039/c1nj20577c

Reference yield:

: 4-(6-(4-(4-methoxy)phenylazo)phenoxy)hexyloxybenzoic acid

: 1346774-35-3
N-(3-(3,5,7,9,11,13,15-heptaisobutyl)pentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propyl-4-(6-(4-(4-methoxy)phenylazo)phenoxy)hexyloxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 8 h / 20 °C / Reflux

2: triethylamine / dichloromethane / 6 h / 0 °C / Reflux

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1039/c1nj20577c