5-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)acetyl)-2-(methoxy)benzoic acid

Base Information

Chemical Name:5-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)acetyl)-2-(methoxy)benzoic acid
CAS No.:1373428-09-1
Molecular Formula:C₂₄H₃₀N₂O₇
Molecular Weight:458.511
Hs Code.:

Synonyms:5-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)acetyl)-2-(methoxy)benzoic acid

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Chemical Property of 5-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)acetyl)-2-(methoxy)benzoic acid

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Technology Process of 5-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)acetyl)-2-(methoxy)benzoic acid

There total 10 articles about 5-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)acetyl)-2-(methoxy)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.6%

: 1373428-00-2
methyl 5-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)acetyl)-2-(methoxy)benzoate

: 1373428-09-1
5-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)acetyl)-2-(methoxy)benzoic acid

Guidance literature:: With potassium carbonate; In methanol; for 1h; Reflux;
DOI:10.1002/cjoc.201180470

Reference yield:

: 500869-36-3
C₁₇H₁₄O₅

: 1373428-09-1
5-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)acetyl)-2-(methoxy)benzoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: bromine / chloroform / 20 °C

2: potassium carbonate / acetonitrile / 20 °C

3: potassium carbonate / methanol / 50 °C

4: thionyl chloride

5: potassium carbonate / acetonitrile / Reflux

6: potassium carbonate / methanol / 1 h / Reflux

With thionyl chloride; bromine; potassium carbonate; In methanol; chloroform; acetonitrile;
DOI:10.1002/cjoc.201180470

Reference yield:

: 1373428-27-3
C₂₃H₂₈N₂O₇

: 1373428-09-1
5-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)acetyl)-2-(methoxy)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride

2: potassium carbonate / acetonitrile / Reflux

3: potassium carbonate / methanol / 1 h / Reflux

With thionyl chloride; potassium carbonate; In methanol; acetonitrile;
DOI:10.1002/cjoc.201180470