Technology Process of C36H50O6
There total 7 articles about C36H50O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diisobutylaluminium hydride;
In
dichloromethane;
at -78 ℃;
DOI:10.1021/ol990567o
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 70 percent / CuCl; TMEDA; air / xylene / 140 °C
2: DIBAL-H / CH2Cl2 / -78 °C
With
air; N,N,N,N,-tetramethylethylenediamine; diisobutylaluminium hydride; copper(l) chloride;
In
dichloromethane; xylene;
1: Glaser oxidation;
DOI:10.1021/ol990567o
- Guidance literature:
-
Multi-step reaction with 4 steps
1: LiBr / tetrahydrofuran / Heating
2: 67 percent / NaH / toluene / Heating
3: 70 percent / CuCl; TMEDA; air / xylene / 140 °C
4: DIBAL-H / CH2Cl2 / -78 °C
With
air; N,N,N,N,-tetramethylethylenediamine; sodium hydride; diisobutylaluminium hydride; copper(l) chloride; lithium bromide;
In
tetrahydrofuran; dichloromethane; toluene; xylene;
3: Glaser oxidation;
DOI:10.1021/ol990567o