Technology Process of C20H27NO2Si
There total 7 articles about C20H27NO2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(l) iodide; diisopropylamine;
bis-triphenylphosphine-palladium(II) chloride;
at 20 ℃;
DOI:10.1016/j.bmcl.2007.03.056
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tetrahydrofuran / -78 °C
1.2: 66 percent / TFA / tetrahydrofuran / -78 °C
2.1: 80 percent / nickel boride; hydrochloric acid / Heating
3.1: 83 percent / I2; silver trifluoromethanesulfonate; HOAc / CH2Cl2 / 20 °C
4.1: 93 percent / toluene / Heating
5.1: 79 percent / Zn; AcOH / 20 °C
6.1: 84 percent / CuI; diisopropylamine / PdCl2(PPh3)2 / 20 °C
With
hydrogenchloride; copper(l) iodide; nickel boride; iodine; silver trifluoromethanesulfonate; acetic acid; diisopropylamine; zinc;
bis-triphenylphosphine-palladium(II) chloride;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2007.03.056
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / nickel boride; hydrochloric acid / Heating
2: 83 percent / I2; silver trifluoromethanesulfonate; HOAc / CH2Cl2 / 20 °C
3: 93 percent / toluene / Heating
4: 79 percent / Zn; AcOH / 20 °C
5: 84 percent / CuI; diisopropylamine / PdCl2(PPh3)2 / 20 °C
With
hydrogenchloride; copper(l) iodide; nickel boride; iodine; silver trifluoromethanesulfonate; acetic acid; diisopropylamine; zinc;
bis-triphenylphosphine-palladium(II) chloride;
In
dichloromethane; toluene;
DOI:10.1016/j.bmcl.2007.03.056