N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycine

Base Information

• Chemical Name: N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycine
• CAS No.: 1022160-17-3
• Molecular Formula: C₄₃H₅₀N₄O₉
• Molecular Weight: 766.891

Synonyms:N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycine

Chemical Property of N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycine

Chemical Property:

Purity/Quality:

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Technology Process of N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycine

There total 2 articles about N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

methyl N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycinate (1022160-16-2) → N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycine (1022160-17-3)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water;

DOI:10.1016/j.tetlet.2008.02.007

Reference yield: 92.0%

tert-butyl N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycinate (1022160-19-5) → N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycine (1022160-17-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane;

DOI:10.1016/j.tetlet.2008.02.007

Reference yield: 91.0%

allyl L-3-(N-acetyl-N-benzyloxy)aminoalaninate (1022160-21-9) + N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycine (1022160-17-3) → allyl N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycinyl-L-3-(N-acetyl-N-benzyloxy)aminoalaninate (1022160-23-1)

Guidance literature:

With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetonitrile; at 20 ℃;

DOI:10.1016/j.tetlet.2008.02.007

upstream raw materials:

methyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate

tert-butyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate

Downstream raw materials:

methyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinyl-L-3-(N-acetyl-N-benzyloxy)aminoalaninate

allyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinyl-L-3-(N-acetyl-N-benzyloxy)aminoalaninate

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