Technology Process of C28H37N5O3Si
There total 10 articles about C28H37N5O3Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C20H19N5O2;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 0 ℃;
for 0.666667h;
2-(tert-butyldimethylsilyloxy)ethyl bromide;
In
N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / water; 1,4-dioxane / 16 h / 110 °C / Inert atmosphere
2.1: sodium hydroxide; hydrogen / ethanol; water; tetrahydrofuran / 40 h / 50 °C / 750.08 Torr
3.1: hydrogenchloride / water; 1,4-dioxane / 3 h / 80 °C
3.2: pH 9
4.1: trichlorophosphate / chloroform / 3 h / Reflux
5.1: propan-1-ol / 16 h / Reflux
6.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.67 h / 0 °C
6.2: 0 - 20 °C
With
hydrogenchloride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; hydrogen; sodium hydride; sodium carbonate; sodium hydroxide; trichlorophosphate;
In
tetrahydrofuran; 1,4-dioxane; propan-1-ol; ethanol; chloroform; water; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride / water; 1,4-dioxane / 3 h / 80 °C
1.2: pH 9
2.1: trichlorophosphate / chloroform / 3 h / Reflux
3.1: propan-1-ol / 16 h / Reflux
4.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.67 h / 0 °C
4.2: 0 - 20 °C
With
hydrogenchloride; sodium hydride; trichlorophosphate;
In
1,4-dioxane; propan-1-ol; chloroform; water; N,N-dimethyl-formamide; mineral oil;