trans-2-Vinylcyclohexylacetic acid

Base Information

Chemical Name:trans-2-Vinylcyclohexylacetic acid
CAS No.:144823-76-7
Molecular Formula:C₁₀H₁₆O₂
Molecular Weight:168.236
Hs Code.:

Synonyms:trans-2-Vinylcyclohexylacetic acid

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Chemical Property of trans-2-Vinylcyclohexylacetic acid

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Technology Process of trans-2-Vinylcyclohexylacetic acid

There total 3 articles about trans-2-Vinylcyclohexylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 144823-75-6
(1RS,6RS,7SR)-6-Dimethyl(phenyl)silyl-4-oxabicyclo<5.4.0>undecan-3-one

: 144823-76-7
trans-2-Vinylcyclohexylacetic acid

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1016/S0040-4020(01)80457-9

Reference yield:

: 144823-78-9
(1RS,5SR,6SR)-5-Dimethyl(phenyl)silylbicyclo<4.4.0>decan-3-one

: 144823-76-7
trans-2-Vinylcyclohexylacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 72 h / Ambient temperature

2: 72 percent / BF₃*Et₂O / CH₂Cl₂ / 3 h / Ambient temperature

With boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/S0040-4020(01)80457-9

Reference yield:

: 144823-77-8
(5RS,6RS)-5-Dimethyl(phenyl)silylbicyclo<4.4.0>dec-1-en-3-one

: 144823-76-7
trans-2-Vinylcyclohexylacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / Li, NH₃ / diethyl ether / 3 h / -78 °C

2: 66 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 72 h / Ambient temperature

3: 72 percent / BF₃*Et₂O / CH₂Cl₂ / 3 h / Ambient temperature

With boron trifluoride diethyl etherate; ammonia; lithium; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)80457-9