phenylmethyl 5-<3-<(methoxycarbonyl)methoxy>phenyl>-4-oxazolecarboxylate

Base Information

Chemical Name:phenylmethyl 5-<3-<(methoxycarbonyl)methoxy>phenyl>-4-oxazolecarboxylate
CAS No.:152576-05-1
Molecular Formula:C₂₀H₁₇NO₆
Molecular Weight:367.358
Hs Code.:

Synonyms:phenylmethyl 5-<3-<(methoxycarbonyl)methoxy>phenyl>-4-oxazolecarboxylate

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Chemical Property of phenylmethyl 5-<3-<(methoxycarbonyl)methoxy>phenyl>-4-oxazolecarboxylate

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Technology Process of phenylmethyl 5-<3-<(methoxycarbonyl)methoxy>phenyl>-4-oxazolecarboxylate

There total 4 articles about phenylmethyl 5-<3-<(methoxycarbonyl)methoxy>phenyl>-4-oxazolecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1738-68-7
Gly-OBz

: 152576-05-1
phenylmethyl 5-<3-<(methoxycarbonyl)methoxy>phenyl>-4-oxazolecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 70 °C

2: POCl₃, Et₃N / CH₂Cl₂ / Ambient temperature

3: 1.) lithium hexamethyldisilazide / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, RT, 5 h

With triethylamine; lithium hexamethyldisilazane; trichlorophosphate; In dichloromethane; toluene;
DOI:10.1021/jm00076a018

Reference yield:

: 51354-16-6
[N-formyl(O-benzyl)]glycinate

: 152576-05-1
phenylmethyl 5-<3-<(methoxycarbonyl)methoxy>phenyl>-4-oxazolecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: POCl₃, Et₃N / CH₂Cl₂ / Ambient temperature

2: 1.) lithium hexamethyldisilazide / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, RT, 5 h

With triethylamine; lithium hexamethyldisilazane; trichlorophosphate; In dichloromethane;
DOI:10.1021/jm00076a018

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 152576-05-1
phenylmethyl 5-<3-<(methoxycarbonyl)methoxy>phenyl>-4-oxazolecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: DCC

2: toluene / 70 °C

3: POCl₃, Et₃N / CH₂Cl₂ / Ambient temperature

4: 1.) lithium hexamethyldisilazide / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, RT, 5 h

With triethylamine; dicyclohexyl-carbodiimide; lithium hexamethyldisilazane; trichlorophosphate; In dichloromethane; toluene;
DOI:10.1021/jm00076a018