10,10'-bis(2-fluorophenyl)-9,9'-bianthracene

Base Information

Chemical Name:10,10'-bis(2-fluorophenyl)-9,9'-bianthracene
CAS No.:1505455-95-7
Molecular Formula:C₄₀H₂₄F₂
Molecular Weight:542.627
Hs Code.:

Synonyms:10,10'-bis(2-fluorophenyl)-9,9'-bianthracene

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Chemical Property of 10,10'-bis(2-fluorophenyl)-9,9'-bianthracene

Chemical Property:

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Technology Process of 10,10'-bis(2-fluorophenyl)-9,9'-bianthracene

There total 3 articles about 10,10'-bis(2-fluorophenyl)-9,9'-bianthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 121848-75-7
10,10'-dibromo-9,9'-bianthryl

: 1993-03-9
o-fluorophenylboronic acid

: 1505455-95-7
10,10'-bis(2-fluorophenyl)-9,9'-bianthracene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; potassium carbonate; In tetrahydrofuran; for 24h; Inert atmosphere; Reflux;
DOI:10.1039/c3tc31743a

Reference yield:

: 84-65-1
9,10-phenanthrenequinone

: 1505455-95-7
10,10'-bis(2-fluorophenyl)-9,9'-bianthracene

Guidance literature:: Multi-step reaction with 3 steps

1: zinc; hydrogenchloride; acetic acid

2: bromine / 1,2-dichloro-ethane

3: water; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran / 24 h / Inert atmosphere; Reflux

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; bromine; potassium carbonate; acetic acid; zinc; In tetrahydrofuran; 1,2-dichloro-ethane; 3: |Suzuki Coupling;
DOI:10.1039/c3tc31743a

Reference yield:

: 1055-23-8
9,9'-bianthracene

: 1505455-95-7
10,10'-bis(2-fluorophenyl)-9,9'-bianthracene

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / 1,2-dichloro-ethane

2: water; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran / 24 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; bromine; potassium carbonate; In tetrahydrofuran; 1,2-dichloro-ethane; 2: |Suzuki Coupling;
DOI:10.1039/c3tc31743a