Technology Process of 1,1,2-trimethyl-2-nitro-3-phenylsulphonylmethylcyclopropane
There total 8 articles about 1,1,2-trimethyl-2-nitro-3-phenylsulphonylmethylcyclopropane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide;
ammonium molybdate;
In
methanol;
for 15h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 98 percent / NaOMe, bromine / methanol; CHCl3 / 1.5 h / -10 °C
2: 72 percent / potassium acetate / ethanol / 15 h / Heating
3: 2 g / bromine, 30 percent potassium hydroxide / H2O / 2 h / 0 °C
4: 74 percent / sulphuric acid / 7 h / Heating
5: 78 percent / LiAlH4 / diethyl ether
6: 0.7 g / pyridine
7: 0.5 g / ethanol / 20 h
8: 92 percent / 30 percent hydrogen peroxide / ammonium molybdate / methanol / 15 h
With
potassium hydroxide; lithium aluminium tetrahydride; sulfuric acid; dihydrogen peroxide; bromine; sodium methylate; potassium acetate;
ammonium molybdate;
In
pyridine; methanol; diethyl ether; ethanol; chloroform; water;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 72 percent / potassium acetate / ethanol / 15 h / Heating
2: 2 g / bromine, 30 percent potassium hydroxide / H2O / 2 h / 0 °C
3: 74 percent / sulphuric acid / 7 h / Heating
4: 78 percent / LiAlH4 / diethyl ether
5: 0.7 g / pyridine
6: 0.5 g / ethanol / 20 h
7: 92 percent / 30 percent hydrogen peroxide / ammonium molybdate / methanol / 15 h
With
potassium hydroxide; lithium aluminium tetrahydride; sulfuric acid; dihydrogen peroxide; bromine; potassium acetate;
ammonium molybdate;
In
pyridine; methanol; diethyl ether; ethanol; water;
