(E)-2-((4-(dimethylamino)phenyl)diazenyl)-N-(3-tert-butyldimethylsiloxypropyl)benzamide

Base Information

Chemical Name:(E)-2-((4-(dimethylamino)phenyl)diazenyl)-N-(3-tert-butyldimethylsiloxypropyl)benzamide
CAS No.:1590361-30-0
Molecular Formula:C₂₄H₃₆N₄O₂Si
Molecular Weight:440.661
Hs Code.:

Synonyms:(E)-2-((4-(dimethylamino)phenyl)diazenyl)-N-(3-tert-butyldimethylsiloxypropyl)benzamide

Suppliers and Price of (E)-2-((4-(dimethylamino)phenyl)diazenyl)-N-(3-tert-butyldimethylsiloxypropyl)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-((4-(dimethylamino)phenyl)diazenyl)-N-(3-tert-butyldimethylsiloxypropyl)benzamide

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Technology Process of (E)-2-((4-(dimethylamino)phenyl)diazenyl)-N-(3-tert-butyldimethylsiloxypropyl)benzamide

There total 1 articles about (E)-2-((4-(dimethylamino)phenyl)diazenyl)-N-(3-tert-butyldimethylsiloxypropyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 74886-84-3
methyl red

: 115306-75-7
3-(tertbutyldimethylsiloxyl)propylamine

: 1590361-30-0
(E)-2-((4-(dimethylamino)phenyl)diazenyl)-N-(3-tert-butyldimethylsiloxypropyl)benzamide

Guidance literature:: With O-(6-chlorobenzo-triazol-1-yl)-N,N,N′,N′-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1021/ja5018442

Reference yield: 100.0%

: 1590361-30-0
(E)-2-((4-(dimethylamino)phenyl)diazenyl)-N-(3-tert-butyldimethylsiloxypropyl)benzamide

: 1590361-32-2
(E)-2-((4-(dimethylamino)phenyl)diazenyl)-N-(3-hydroxypropyl)benzamide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 5h; Inert atmosphere;
DOI:10.1021/ja5018442

Reference yield:

: 1590361-30-0
(E)-2-((4-(dimethylamino)phenyl)diazenyl)-N-(3-tert-butyldimethylsiloxypropyl)benzamide

: C₂₅H₂₅BF₃N₄O₃^(1-)*K⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere

2: sodium hydride / dimethyl sulfoxide; mineral oil / 16 h / 20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; dimethyl sulfoxide; mineral oil;
DOI:10.1021/ja5018442