{(trimethylsilylmethylene)(2,6-diisopropylphenylimido)((OC(CH₃)(CF₃)2)2) molybdenum

Base Information

• Chemical Name: {(trimethylsilylmethylene)(2,6-diisopropylphenylimido)((OC(CH₃)(CF₃)2)2) molybdenum
• CAS No.: 108945-99-9
• Molecular Formula: C₂₄H₃₃F₁₂MoNO₂Si
• Molecular Weight: 719.538

Synonyms:{(trimethylsilylmethylene)(2,6-diisopropylphenylimido)((OC(CH₃)(CF₃)2)2) molybdenum

Chemical Property of {(trimethylsilylmethylene)(2,6-diisopropylphenylimido)((OC(CH₃)(CF₃)2)2) molybdenum

Chemical Property:

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Technology Process of {(trimethylsilylmethylene)(2,6-diisopropylphenylimido)((OC(CH₃)(CF₃)2)2) molybdenum

There total 4 articles about {(trimethylsilylmethylene)(2,6-diisopropylphenylimido)((OC(CH₃)(CF₃)2)2) molybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

{(neopentylidene)(2,6-diisopropylphenylimido)((OC(CH3)(CF3)2)2) molybdenum} (108945-98-8,153483-68-2,153483-76-2) + ethenyltrimethylsilane (754-05-2) → {(trimethylsilylmethylene)(2,6-diisopropylphenylimido)((OC(CH3)(CF3)2)2) molybdenum (108945-99-9)

Guidance literature:

In pentane; byproducts: neohexene; Mo-compd. is dissolved in pentane and vinyltrimethylsilane is added (-30°C), soln. is allowed to warm to room temp. over 2.5 h; evapn., recrystn. from pentane (-40°C), elem. anal.;

DOI:10.1021/ja00166a023

Reference yield: 74.0%

Mo(CH-t-Bu)(=N-2,6-diisopropylphenyl){OCMe(CF3)2}2 (108945-98-8,153483-76-2,153483-68-2) + ethenyltrimethylsilane (754-05-2) → {(trimethylsilylmethylene)(2,6-diisopropylphenylimido)((OC(CH3)(CF3)2)2) molybdenum (108945-99-9)

Guidance literature:

In pentane; Me3SiCH=CH2 was added all at once to an ether soln. of Mo-complex at -30°C, soln. was allowed to warm to room temp. over 2.5 h; evapd., residue was recrystd. from pentane at -40°C;

DOI:10.1021/om00149a048

Reference yield:

(neopentylidene)(2,6-diisopropylphenylimido)(1,2-dimethoxy-ethane)(Cl)2 molybdenum → {(trimethylsilylmethylene)(2,6-diisopropylphenylimido)((OC(CH3)(CF3)2)2) molybdenum (108945-99-9)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: pentane

In diethyl ether; pentane;

DOI:10.1021/ja00166a023

upstream raw materials:

{(neopentylidene)(2,6-diisopropylphenylimido)((OC(CH₃)(CF₃)2)2) molybdenum}

ethenyltrimethylsilane

Mo(CH-t-Bu)(=N-2,6-diisopropylphenyl){OCMe(CF₃)2}2

Mo(CHC(CH₃)3)(NC₆H₃(CH(CH₃)2)2)Cl₂

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