3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-threonine methyl ester

Base Information

Chemical Name:3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-threonine methyl ester
CAS No.:74112-78-0
Molecular Formula:C₂₅H₃₄N₂O₁₂
Molecular Weight:554.551
Hs Code.:

Synonyms:3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-threonine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-threonine methyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-threonine methyl ester

There total 6 articles about 3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-threonine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-O-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-threonine methyl ester

: 3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-L-threonine methyl ester

: 74112-78-0
3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-threonine methyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 7h; under 760 Torr; Title compound not separated from byproducts;
DOI:10.1016/S0008-6215(00)85142-3

Reference yield:

: 67817-37-2
3,4,6-tri-O-acetyl-2-azido-2-deoxy-β-D-galactopyranosyl chloride

: 74112-78-0
3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-threonine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / mercuric cyanide, mercuric chloride / nitromethane / 24 h / 70 °C

2: H₂ / 5 percent Pd/C / methanol / 7 h / 760 Torr

With hydrogen; mercury(II) cyanide; mercury dichloride; palladium on activated charcoal; In methanol; nitromethane;
DOI:10.1016/S0008-6215(00)85142-3

Reference yield:

: 57224-63-2,62076-80-6,84449-06-9,98777-33-4,98777-34-5,100157-53-7
N-(benzyloxycarbonyl)-L-threonine methyl ester

: 74112-78-0
3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-threonine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / mercuric cyanide, mercuric chloride / nitromethane / 24 h / 70 °C

2: H₂ / 5 percent Pd/C / methanol / 7 h / 760 Torr

With hydrogen; mercury(II) cyanide; mercury dichloride; palladium on activated charcoal; In methanol; nitromethane;
DOI:10.1016/S0008-6215(00)85142-3