Technology Process of C26H31N5O3S
There total 8 articles about C26H31N5O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 30 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: dmap; triethylamine / tetrahydrofuran / 16 h / 30 °C
2.1: hydrogen / palladium on activated charcoal / tetrahydrofuran / 16 h / 40 °C / 2585.81 Torr
3.1: triethylamine / DCE / 1 h / 30 °C
3.2: 16 h / 30 °C
4.1: hydrogen / palladium on activated charcoal / methanol / 16 h / 40 °C / 2585.81 Torr
5.1: triethylamine; sodium tris(acetoxy)borohydride / DCE / 16 h / 30 °C
6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 16 h / 30 °C
7.1: trifluoroacetic acid / dichloromethane / 16 h / 30 °C
With
dmap; hydrogen; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; DCE; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen / palladium on activated charcoal / methanol / 16 h / 40 °C / 2585.81 Torr
2: triethylamine; sodium tris(acetoxy)borohydride / DCE / 16 h / 30 °C
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 16 h / 30 °C
4: trifluoroacetic acid / dichloromethane / 16 h / 30 °C
With
hydrogen; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
palladium on activated charcoal;
In
methanol; DCE; dichloromethane; acetonitrile;