Technology Process of C58H71NO9
There total 5 articles about C58H71NO9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; dicyclohexyl-carbodiimide;
In
dichloromethane;
at 20 ℃;
for 24h;
DOI:10.3762/bjoc.8.15
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C
2: dihydrogen peroxide; acetic acid / water / 22 h / 40 - 75 °C
3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C
4: 10 wt % palladium on activated carbon; hydrogen / ethyl acetate / 760.05 Torr
5: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C
With
dmap; 10 wt % palladium on activated carbon; hydrogen; dihydrogen peroxide; acetic acid; dicyclohexyl-carbodiimide;
In
dichloromethane; water; ethyl acetate;
DOI:10.3762/bjoc.8.15
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dihydrogen peroxide; acetic acid / water / 22 h / 40 - 75 °C
2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C
3: 10 wt % palladium on activated carbon; hydrogen / ethyl acetate / 760.05 Torr
4: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C
With
dmap; 10 wt % palladium on activated carbon; hydrogen; dihydrogen peroxide; acetic acid; dicyclohexyl-carbodiimide;
In
dichloromethane; water; ethyl acetate;
DOI:10.3762/bjoc.8.15
