2-(1,4-dioxa-5-cyclopentyl)-4-guanidinophenol

Base Information

Chemical Name:2-(1,4-dioxa-5-cyclopentyl)-4-guanidinophenol
CAS No.:624722-40-3
Molecular Formula:C₁₀H₁₃N₃O₃
Molecular Weight:223.232
Hs Code.:

Synonyms:2-(1,4-dioxa-5-cyclopentyl)-4-guanidinophenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(1,4-dioxa-5-cyclopentyl)-4-guanidinophenol

Chemical Property:

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Technology Process of 2-(1,4-dioxa-5-cyclopentyl)-4-guanidinophenol

There total 4 articles about 2-(1,4-dioxa-5-cyclopentyl)-4-guanidinophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 624722-39-0
4-[N',N''-bis(benzyloxycarbonyl)guanidino]-2-(1,4-dioxa-5-cyclopentyl)phenol

: 624722-40-3
2-(1,4-dioxa-5-cyclopentyl)-4-guanidinophenol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; water; at 20 ℃; for 1h;
DOI:10.1248/cpb.51.625

Reference yield:

: 22068-55-9
2-(1,4-dioxa-5-cyclopentyl)-4-nitrophenol

: 624722-40-3
2-(1,4-dioxa-5-cyclopentyl)-4-guanidinophenol

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / H₂ / Pd/C / dioxane; ethanol / 1 h / 20 °C

2: 90 percent / tetrahydrofuran / 1 h / 20 °C

3: 87 percent / H₂ / Pd/C / ethanol; H₂O / 1 h / 20 °C

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; ethanol; water;
DOI:10.1248/cpb.51.625

Reference yield:

: 97-51-8
5-Nitrosalicylaldehyde

: 624722-40-3
2-(1,4-dioxa-5-cyclopentyl)-4-guanidinophenol

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / p-TsOH / benzene / 4 h / Heating

2: 89 percent / H₂ / Pd/C / dioxane; ethanol / 1 h / 20 °C

3: 90 percent / tetrahydrofuran / 1 h / 20 °C

4: 87 percent / H₂ / Pd/C / ethanol; H₂O / 1 h / 20 °C

With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; ethanol; water; benzene;
DOI:10.1248/cpb.51.625