Technology Process of (Z)-3-(3-propoxyphenyl)acrylic acid
There total 3 articles about (Z)-3-(3-propoxyphenyl)acrylic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / acetone / 0.25 h / 0 °C / Inert atmosphere
1.2: 6 h / Inert atmosphere; Reflux
2.1: N-benzyl-trimethylammonium hydroxide / methanol; tetrahydrofuran / -78 °C / Inert atmosphere
2.2: -78 °C / Inert atmosphere
3.1: sodium hydroxide; water / ethanol / 4 h / 20 °C
With
water; N-benzyl-trimethylammonium hydroxide; potassium carbonate; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; acetone;
2.1: |Horner-Wadsworth-Emmons Olefination / 2.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.phytochem.2013.08.013
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-benzyl-trimethylammonium hydroxide / methanol; tetrahydrofuran / -78 °C / Inert atmosphere
1.2: -78 °C / Inert atmosphere
2.1: sodium hydroxide; water / ethanol / 4 h / 20 °C
With
water; N-benzyl-trimethylammonium hydroxide; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol;
1.1: |Horner-Wadsworth-Emmons Olefination / 1.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.phytochem.2013.08.013