(+/-)-N-(tert-butoxycarbonyl)-3-O-(tert-butyldimethylsilyl)-2-benzylserine

Base Information

Chemical Name:(+/-)-N-(tert-butoxycarbonyl)-3-O-(tert-butyldimethylsilyl)-2-benzylserine
CAS No.:171898-30-9
Molecular Formula:C₂₁H₃₅NO₅Si
Molecular Weight:409.598
Hs Code.:

Synonyms:(+/-)-N-(tert-butoxycarbonyl)-3-O-(tert-butyldimethylsilyl)-2-benzylserine

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Chemical Property of (+/-)-N-(tert-butoxycarbonyl)-3-O-(tert-butyldimethylsilyl)-2-benzylserine

Chemical Property:

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Technology Process of (+/-)-N-(tert-butoxycarbonyl)-3-O-(tert-butyldimethylsilyl)-2-benzylserine

There total 5 articles about (+/-)-N-(tert-butoxycarbonyl)-3-O-(tert-butyldimethylsilyl)-2-benzylserine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 171898-30-9
(+/-)-N-(tert-butoxycarbonyl)-3-O-(tert-butyldimethylsilyl)-2-benzylserine

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / 2,6-dimethylpyridine / CH₂Cl₂ / 1 h / Ambient temperature

2: 1.) SnCl₄, 2.) imidazole / 1.) Et₂O, -80 deg C, 2 h, 2.) DMF, room temp., 20 h

3: KMnO₄, dicyclohexano-18-crown-6 ether / CH₂Cl₂ / 2 h / Ambient temperature

With 1H-imidazole; 2,6-dimethylpyridine; perhydrodibenzo-18-crown-6; potassium permanganate; tin(IV) chloride; In dichloromethane;

Reference yield:

: 141293-28-9
N-(tert-butoxycarbonyl)-2-[(tert-butyldimethylsilyl)oxy]pyrrole

: 171898-30-9
(+/-)-N-(tert-butoxycarbonyl)-3-O-(tert-butyldimethylsilyl)-2-benzylserine

Guidance literature:: Multi-step reaction with 5 steps

1: 60 percent / SnCl₄ / diethyl ether / 2 h / -80 °C

2: 98 percent / 2,6-dimethylpyridine / CH₂Cl₂ / 1 h / Ambient temperature

3: 58 percent / CF₃CO₂H / CH₂Cl₂ / 2 h / 0 °C

4: KMnO₄, dicyclohexano-18-crown-6 ether / CH₂Cl₂ / 2 h / Ambient temperature

With 2,6-dimethylpyridine; perhydrodibenzo-18-crown-6; potassium permanganate; tin(IV) chloride; trifluoroacetic acid; In diethyl ether; dichloromethane;

Reference yield:

: 171898-25-2
5-benzyl-N-(tert-butoxycarbonyl)-2-(tert-butyldimethylsiloxy)pyrrole

: 171898-30-9
(+/-)-N-(tert-butoxycarbonyl)-3-O-(tert-butyldimethylsilyl)-2-benzylserine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) SnCl₄, 2.) imidazole / 1.) Et₂O, -80 deg C, 2 h, 2.) DMF, room temp., 20 h

2: KMnO₄, dicyclohexano-18-crown-6 ether / CH₂Cl₂ / 2 h / Ambient temperature

With 1H-imidazole; perhydrodibenzo-18-crown-6; potassium permanganate; tin(IV) chloride; In dichloromethane;