Benzyl 2-acetamido-6-O-benzoyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside

Base Information

Chemical Name:Benzyl 2-acetamido-6-O-benzoyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside
CAS No.:120484-41-5
Molecular Formula:C₂₅H₂₉NO₉
Molecular Weight:487.507
Hs Code.:

Synonyms:Benzyl 2-acetamido-6-O-benzoyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside

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Chemical Property of Benzyl 2-acetamido-6-O-benzoyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside

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Technology Process of Benzyl 2-acetamido-6-O-benzoyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside

There total 4 articles about Benzyl 2-acetamido-6-O-benzoyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 613-90-1
benzoyl cyanide

: 127528-39-6
Benzyl 2-acetamido-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside

: 120484-41-5
Benzyl 2-acetamido-6-O-benzoyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside

Guidance literature:: With triethylamine; In dichloromethane; at 5 ℃; for 12h;

Reference yield:

: 66026-10-6
N-((4aR,6S,7R,8R,8aS)-6-(benzyloxy)-8-hydroxy-2,2-dimethylhexahydropyrano[3,2-d][1,3]dioxin-7-yl)acetamide

: 120484-41-5
Benzyl 2-acetamido-6-O-benzoyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Sodium hydride / 1.) Dioxane, 90 deg C, 2 h, 2.) 65 deg C, 6 h, 3.) ethyl acetate, ether, room temperature, 30 min.

2: 73.6 percent / Dowex 50 (H⁺-form) / methanol / 2 h / Reflux

3: 67 percent / Triethylamine / CH₂Cl₂ / 12 h / 5 °C

With Dowex 50 (H⁺-form); sodium hydride; triethylamine; In methanol; dichloromethane;

Reference yield:

: 127528-38-5
benzyl-2-acetamino-2-deoxy-4,6-O-isopropylidene-3-O-methoxycarbonylmethyl-α-D-glucopyranoside

: 120484-41-5
Benzyl 2-acetamido-6-O-benzoyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 73.6 percent / Dowex 50 (H⁺-form) / methanol / 2 h / Reflux

2: 67 percent / Triethylamine / CH₂Cl₂ / 12 h / 5 °C

With Dowex 50 (H⁺-form); triethylamine; In methanol; dichloromethane;