(2S,3S)-<<2-(Methoxymethoxy)-3-methyl-5-(phenylsulfonyl)-1-pentyl>oxy>(1,1-dimethylethyl)diphenylsilane

Base Information

Chemical Name:(2S,3S)-<<2-(Methoxymethoxy)-3-methyl-5-(phenylsulfonyl)-1-pentyl>oxy>(1,1-dimethylethyl)diphenylsilane
CAS No.:152033-06-2
Molecular Formula:C₃₀H₄₀O₅SSi
Molecular Weight:540.796
Hs Code.:

Synonyms:(2S,3S)-<<2-(Methoxymethoxy)-3-methyl-5-(phenylsulfonyl)-1-pentyl>oxy>(1,1-dimethylethyl)diphenylsilane

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Chemical Property of (2S,3S)-<<2-(Methoxymethoxy)-3-methyl-5-(phenylsulfonyl)-1-pentyl>oxy>(1,1-dimethylethyl)diphenylsilane

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Technology Process of (2S,3S)-<<2-(Methoxymethoxy)-3-methyl-5-(phenylsulfonyl)-1-pentyl>oxy>(1,1-dimethylethyl)diphenylsilane

There total 6 articles about (2S,3S)-<<2-(Methoxymethoxy)-3-methyl-5-(phenylsulfonyl)-1-pentyl>oxy>(1,1-dimethylethyl)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 165961-38-6
(2S,3S)-<<2-(Methoxymethoxy)-3-methyl-5-(phenylthio)-1-pentyl>oxy>(1,1-dimethylethyl)diphenylsilane

: 152033-06-2
(2S,3S)-<<2-(Methoxymethoxy)-3-methyl-5-(phenylsulfonyl)-1-pentyl>oxy>(1,1-dimethylethyl)diphenylsilane

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/S0040-4039(00)74091-3

Reference yield:

: 115869-43-7
(tert-butyldiphenylsilanyloxy)acetaldehyde

: 152033-06-2
(2S,3S)-<<2-(Methoxymethoxy)-3-methyl-5-(phenylsulfonyl)-1-pentyl>oxy>(1,1-dimethylethyl)diphenylsilane

Guidance literature:: Multi-step reaction with 5 steps

1: 2) H₂O₂, NaOH / 1) THF, -78 deg C

2: i-Pr₂NEt / CH₂Cl₂

3: 1) 9-BBN, 2) H₂O₂, NaOH / 1) THF, 15 deg C

4: 92 percent / n-Bu₃P / pyridine

5: 100 percent / m-CPBA / CH₂Cl₂

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; tributylphosphine; dihydrogen peroxide; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In pyridine; dichloromethane;
DOI:10.1016/S0040-4039(00)74091-3

Reference yield:

: 165961-37-5
(3S,4S)-4-(Methoxymethoxy)-3-methyl-5-<<(1,1-dimethylethyl)diphenylsilyl>oxy>-1-pentanol

: 152033-06-2
(2S,3S)-<<2-(Methoxymethoxy)-3-methyl-5-(phenylsulfonyl)-1-pentyl>oxy>(1,1-dimethylethyl)diphenylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / n-Bu₃P / pyridine

2: 100 percent / m-CPBA / CH₂Cl₂

With tributylphosphine; 3-chloro-benzenecarboperoxoic acid; In pyridine; dichloromethane;
DOI:10.1016/S0040-4039(00)74091-3