(E)-ethyl 3-(N-(3-diazo-2-oxopropyl)-4-methylphenylsulfonamido)acrylate

Base Information

Chemical Name:(E)-ethyl 3-(N-(3-diazo-2-oxopropyl)-4-methylphenylsulfonamido)acrylate
CAS No.:1361127-66-3
Molecular Formula:C₁₅H₁₇N₃O₅S
Molecular Weight:351.383
Hs Code.:

Synonyms:(E)-ethyl 3-(N-(3-diazo-2-oxopropyl)-4-methylphenylsulfonamido)acrylate

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Chemical Property of (E)-ethyl 3-(N-(3-diazo-2-oxopropyl)-4-methylphenylsulfonamido)acrylate

Chemical Property:

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Technology Process of (E)-ethyl 3-(N-(3-diazo-2-oxopropyl)-4-methylphenylsulfonamido)acrylate

There total 4 articles about (E)-ethyl 3-(N-(3-diazo-2-oxopropyl)-4-methylphenylsulfonamido)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1361126-83-1
(E)-2-(N-(3-ethoxy-3-oxoprop-1-enyl)-4-methylphenylsulfonamido)acetic acid

: 1361127-66-3
(E)-ethyl 3-(N-(3-diazo-2-oxopropyl)-4-methylphenylsulfonamido)acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane / 2 h / 25 °C

2: diethyl ether / 2 h / 0 - 25 °C

With oxalyl dichloride; In diethyl ether; dichloromethane;
DOI:10.1039/c2ob06591f

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1361127-66-3
(E)-ethyl 3-(N-(3-diazo-2-oxopropyl)-4-methylphenylsulfonamido)acrylate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / water / 60 °C

2: 1,4-diaza-bicyclo[2.2.2]octane / dichloromethane

3: oxalyl dichloride / dichloromethane / 2 h / 25 °C

4: diethyl ether / 2 h / 0 - 25 °C

With 1,4-diaza-bicyclo[2.2.2]octane; oxalyl dichloride; sodium hydroxide; In diethyl ether; dichloromethane; water;
DOI:10.1039/c2ob06591f

Reference yield:

: 1080-44-0
N-Tosylglycine

: 1361127-66-3
(E)-ethyl 3-(N-(3-diazo-2-oxopropyl)-4-methylphenylsulfonamido)acrylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1,4-diaza-bicyclo[2.2.2]octane / dichloromethane

2: oxalyl dichloride / dichloromethane / 2 h / 25 °C

3: diethyl ether / 2 h / 0 - 25 °C

With 1,4-diaza-bicyclo[2.2.2]octane; oxalyl dichloride; In diethyl ether; dichloromethane;
DOI:10.1039/c2ob06591f