Technology Process of C15H18O3
There total 3 articles about C15H18O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
methanol;
at 20 ℃;
for 3h;
Sealed vial;
Inert atmosphere;
DOI:10.1021/ja203171x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: C46H32F12FeP2; diethoxymethylane; copper(II) acetate monohydrate; tert-butyl alcohol / toluene / 0 - 4 °C / Sealed vial; Inert atmosphere
2: potassium carbonate / methanol / 3 h / 20 °C / Sealed vial; Inert atmosphere
With
diethoxymethylane; C46H32F12FeP2; copper(II) acetate monohydrate; potassium carbonate; tert-butyl alcohol;
In
methanol; toluene;
DOI:10.1021/ja203171x
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium diacetate; tris(2,6-dimethoxyphenyl)phosphine / toluene / 18 h / 20 °C
2: C46H32F12FeP2; diethoxymethylane; copper(II) acetate monohydrate; tert-butyl alcohol / toluene / 0 - 4 °C / Sealed vial; Inert atmosphere
3: potassium carbonate / methanol / 3 h / 20 °C / Sealed vial; Inert atmosphere
With
diethoxymethylane; C46H32F12FeP2; palladium diacetate; copper(II) acetate monohydrate; potassium carbonate; tris(2,6-dimethoxyphenyl)phosphine; tert-butyl alcohol;
In
methanol; toluene;
DOI:10.1021/ja203171x