C₂₆H₂₈N₂O₃

Base Information

Chemical Name:C₂₆H₂₈N₂O₃
CAS No.:1572572-02-1
Molecular Formula:C₂₆H₂₈N₂O₃
Molecular Weight:416.52
Hs Code.:

C<sub>26</sub>H<sub>28</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₆H₂₈N₂O₃

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Chemical Property of C₂₆H₂₈N₂O₃

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Technology Process of C₂₆H₂₈N₂O₃

There total 8 articles about C₂₆H₂₈N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1572571-98-2
C₂₆H₂₆N₂O₂

: 1572572-02-1
C₂₆H₂₈N₂O₃

Guidance literature:: With formic acid; at 20 ℃;
DOI:10.1021/jo402741g

Reference yield:

: 90-04-0
2-methoxy-phenylamine

: 1572572-02-1
C₂₆H₂₈N₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene-4-sulfonic acid / toluene

2.1: palladium diacetate; copper diacetate; potassium carbonate / N,N-dimethyl-formamide / 3 h / 140 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 20 °C

3.2: 2 h / 0 - 20 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

4.2: 1 h / -78 °C / Inert atmosphere

5.1: potassium tert-butylate / tetrahydrofuran; tert-butyl alcohol / 0.17 h / 0 °C

5.2: 0.05 h / 0 °C

6.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol / toluene / 12 h / 20 - 70 °C / Inert atmosphere

7.1: formic acid / 20 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; formic acid; potassium tert-butylate; copper diacetate; palladium diacetate; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; mineral oil; tert-butyl alcohol;
DOI:10.1021/jo402741g

Reference yield:

: 504-02-9
1,3-cylohexanedione

: 1572572-02-1
C₂₆H₂₈N₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene-4-sulfonic acid / toluene

2.1: palladium diacetate; copper diacetate; potassium carbonate / N,N-dimethyl-formamide / 3 h / 140 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 20 °C

3.2: 2 h / 0 - 20 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

4.2: 1 h / -78 °C / Inert atmosphere

5.1: potassium tert-butylate / tetrahydrofuran; tert-butyl alcohol / 0.17 h / 0 °C

5.2: 0.05 h / 0 °C

6.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol / toluene / 12 h / 20 - 70 °C / Inert atmosphere

7.1: formic acid / 20 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; formic acid; potassium tert-butylate; copper diacetate; palladium diacetate; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; mineral oil; tert-butyl alcohol;
DOI:10.1021/jo402741g