diisopropoxyborane

Base Information

• Chemical Name: diisopropoxyborane
• CAS No.: 13990-97-1
• Molecular Formula: C₆H₁₅BO₂
• Molecular Weight: 129.995

Synonyms:diisopropoxyborane

Chemical Property of diisopropoxyborane

Chemical Property:

Purity/Quality:

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Technology Process of diisopropoxyborane

There total 1 articles about diisopropoxyborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

borane-THF (14044-65-6) + Ti(OiPr)[{(O-2,4-Me2C6H2)-6-CH2}3N] (350484-87-6) → diisopropoxyborane (13990-97-1) + [Ti(η3-tetrahydroborate)((OC6Me2H2CH2)3N)]*toluene (1001404-47-2)

Guidance literature:

In not given; (Ar); addn. of excess of boron compd. to soln. of titanium compd.; (11)B NMR;

DOI:10.1039/b708378e

Reference yield:

diisopropoxyborane (13990-97-1) → metaboric acid (13460-50-9) + isopropyl alcohol (67-63-0,8013-70-5)

Guidance literature:

Hydrolysis;

Reference yield:

diisopropoxyborane (13990-97-1) + potassium hydride → potassium tri(isopropoxy)borohydride + potassium monoisopropoxyborohydride + K-tetrakis(isopropoxy)borate

Guidance literature:

In tetrahydrofuran; diisopropoxyborane treated with KH in THF at 0°C;

DOI:10.1021/om00077a011

upstream raw materials:

borane-THF

Ti(OⁱPr)[{(O-2,4-Me₂C₆H₂)-6-CH₂}₃N]

Downstream raw materials:

metaboric acid

isopropyl alcohol

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