5-Bromo-2-(bromomethyl)-1,3-benzothiazole

Base Information

Chemical Name:5-Bromo-2-(bromomethyl)-1,3-benzothiazole
CAS No.:110704-13-7
Molecular Formula:C₈H₅Br₂NS
Molecular Weight:307.008
Hs Code.:
DSSTox Substance ID:DTXSID80560591
Wikidata:Q82444019
Mol file:110704-13-7.mol

Synonyms:110704-13-7;5-Bromo-2-(bromomethyl)-1,3-benzothiazole;5-BROMO-2-(BROMOMETHYL)BENZOTHIAZOLE;SCHEMBL201370;DTXSID80560591;JEMIBNMZWVIQHH-UHFFFAOYSA-N;2-Bromomethyl-5-bromobenzothiazole;5-bromo-2-bromomethylbenzothiazole;5-bromo-2-bromomethyl-benzothiazole;5-Bromo-2-(bromomethyl)benzo[d]thiazole

Suppliers and Price of 5-Bromo-2-(bromomethyl)-1,3-benzothiazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 5-Bromo-2-(bromomethyl)-1,3-benzothiazole

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:306.84890
Heavy Atom Count:12
Complexity:167

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C(C=C1Br)N=C(S2)CBr

Technology Process of 5-Bromo-2-(bromomethyl)-1,3-benzothiazole

There total 5 articles about 5-Bromo-2-(bromomethyl)-1,3-benzothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 63837-11-6
5-bromo-2-methylbenzothiazole

: 110704-13-7
2-(bromomethyl)-5-bromobenzothiazole

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 24h; Heating / reflux;

Reference yield:

: 123-56-8,89963-74-6
Succinimide

: 110704-13-7
2-(bromomethyl)-5-bromobenzothiazole

Guidance literature:

Reference yield:

: 25462-66-2
N-(2,5-dibromophenyl)acetamide

: 110704-13-7
2-(bromomethyl)-5-bromobenzothiazole

Guidance literature:: Multi-step reaction with 3 steps

1: 29 percent / P₄S₁₀ / benzene / 18 h / Heating

2: 49 percent / N-methylpyrrolidinone, NaH / 1.5 h / 150 °C

3: 23 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 14 h / Heating; Irradiation

With 1-methyl-pyrrolidin-2-one; N-Bromosuccinimide; Perbenzoic acid; tetraphosphorus decasulfide; sodium hydride; In tetrachloromethane; benzene;
DOI:10.1021/jm00105a018