1,1-dimethylethyl-3-fluoro-3-[(4-fluorophenyl)carbonyl]-1-piperidinecarboxylate

Base Information

Chemical Name:1,1-dimethylethyl-3-fluoro-3-[(4-fluorophenyl)carbonyl]-1-piperidinecarboxylate
CAS No.:645379-37-9
Molecular Formula:C₁₇H₂₁F₂NO₃
Molecular Weight:325.355
Hs Code.:

Synonyms:1,1-dimethylethyl-3-fluoro-3-[(4-fluorophenyl)carbonyl]-1-piperidinecarboxylate

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Chemical Property of 1,1-dimethylethyl-3-fluoro-3-[(4-fluorophenyl)carbonyl]-1-piperidinecarboxylate

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Technology Process of 1,1-dimethylethyl-3-fluoro-3-[(4-fluorophenyl)carbonyl]-1-piperidinecarboxylate

There total 1 articles about 1,1-dimethylethyl-3-fluoro-3-[(4-fluorophenyl)carbonyl]-1-piperidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 639468-31-8
3-(4-fluorobenzoyl)piperidine-1-carboxylic acid tert-butyl ester

: 645379-37-9
1,1-dimethylethyl-3-fluoro-3-[(4-fluorophenyl)carbonyl]-1-piperidinecarboxylate

Guidance literature:: 3-(4-fluorobenzoyl)piperidine-1-carboxylic acid tert-butyl ester; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - -10 ℃; for 1h;

With N-fluorobis(benzenesulfon)imide; In tetrahydrofuran; at -40 - 20 ℃; for 1h;

Reference yield:

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 645379-37-9
1,1-dimethylethyl-3-fluoro-3-[(4-fluorophenyl)carbonyl]-1-piperidinecarboxylate

: 645379-38-0
1,1-dimethylethyl-3-[3-(ethyloxy)-1-(4-fluorophenyl)-3-oxo-1-propen-1-yl]-3-fluoro-1-piperidinecarboxylate

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 0.333333h;

1,1-dimethylethyl-3-fluoro-3-[(4-fluorophenyl)carbonyl]-1-piperidinecarboxylate; In tetrahydrofuran; mineral oil; for 2h; Heating / reflux;