1,2-O-isopropylidene-3-O-benzyl-5,6,7-trideoxy-5,7-(N-benzylimino)-β-L-ido-sept-1,4-furanose

Base Information

Chemical Name:1,2-O-isopropylidene-3-O-benzyl-5,6,7-trideoxy-5,7-(N-benzylimino)-β-L-ido-sept-1,4-furanose
CAS No.:1240486-41-2
Molecular Formula:C₂₄H₂₉NO₄
Molecular Weight:395.499
Hs Code.:

Synonyms:1,2-O-isopropylidene-3-O-benzyl-5,6,7-trideoxy-5,7-(N-benzylimino)-β-L-ido-sept-1,4-furanose

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Chemical Property of 1,2-O-isopropylidene-3-O-benzyl-5,6,7-trideoxy-5,7-(N-benzylimino)-β-L-ido-sept-1,4-furanose

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Technology Process of 1,2-O-isopropylidene-3-O-benzyl-5,6,7-trideoxy-5,7-(N-benzylimino)-β-L-ido-sept-1,4-furanose

There total 5 articles about 1,2-O-isopropylidene-3-O-benzyl-5,6,7-trideoxy-5,7-(N-benzylimino)-β-L-ido-sept-1,4-furanose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1240486-39-8
1,2-O-isopropylidene-3-O-benzyl-5,6-dideoxy-5,7-(N-benzylimino)-β-L-ido-sept-1,4-furan-7-ulose

: 1240486-41-2
1,2-O-isopropylidene-3-O-benzyl-5,6,7-trideoxy-5,7-(N-benzylimino)-β-L-ido-sept-1,4-furanose

Guidance literature:: With aluminum (III) chloride; lithium aluminium tetrahydride; In tetrahydrofuran; at -10 - 0 ℃; for 0.25h; Inert atmosphere;
DOI:10.1039/c004690f

Reference yield: 72.0%

: 328313-31-1
3-O-benzyl-5,6-dideoxy-5-(N-benzyl)amino-1,2-O-isopropylidene-β-L-ido-hepto-1,4-furanose

: 1240486-41-2
1,2-O-isopropylidene-3-O-benzyl-5,6,7-trideoxy-5,7-(N-benzylimino)-β-L-ido-sept-1,4-furanose

Guidance literature:: With [bis(acetoxy)iodo]benzene; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 10h; Time; Reagent/catalyst;
DOI:10.1039/c3ra23467c

Reference yield:

: 100-46-9
benzylamine

: 1240486-41-2
1,2-O-isopropylidene-3-O-benzyl-5,6,7-trideoxy-5,7-(N-benzylimino)-β-L-ido-sept-1,4-furanose

Guidance literature:: Multi-step reaction with 3 steps

1: N-methylmorpholinium hydrogen sulphate / ethanol / 0.25 h / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 20 °C

3: triphenylphosphine; di-isopropyl azodicarboxylate; [bis(acetoxy)iodo]benzene / tetrahydrofuran / 10 h / 20 °C

With lithium aluminium tetrahydride; [bis(acetoxy)iodo]benzene; di-isopropyl azodicarboxylate; N-methylmorpholinium hydrogen sulphate; triphenylphosphine; In tetrahydrofuran; ethanol; 3: |Mitsunobu Displacement;
DOI:10.1039/c3ra23467c