4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline

Base Information

• Chemical Name: 4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline
• CAS No.: 1338083-03-6
• Molecular Formula: C₄₂H₆₅NO₂Sn
• Molecular Weight: 734.694
• Mol file: 1338083-03-6.mol

Synonyms:4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline

Chemical Property of 4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline

There total 1 articles about 4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-bis(4-hexyloxyphenyl)-4-bromophenylamine (1092363-75-1) + tributyltin chloride (1461-22-9) → 4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline (1338083-03-6)

Guidance literature:

N,N-bis(4-hexyloxyphenyl)-4-bromophenylamine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2h;

tributyltin chloride; In tetrahydrofuran; hexane;

DOI:10.1021/ol301730c

Reference yield: 87.0%

4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline (1338083-03-6) + 5-(2,3-bis(3,4-bis(hexyloxy)phenyl)-8-(5-bromothiophen-2-yl)quinoxalin-5-yl)thiophene-2-carbaldehyde → 5-(8-(5-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)thiophen-2-yl)-2,3-bis(3,4-bis(hexyloxy)phenyl)quinoxalin-5-yl)thiophene-2-carbaldehyde

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 100 ℃; for 15h; Schlenk technique; Inert atmosphere;

DOI:10.1039/c8ta04774j

Reference yield: 80.0%

4-(hexyloxy)-N-(4-(hexyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline (1338083-03-6) + 5-(2,3-bis(3,4-bis(hexyloxy)phenyl)-7-(5-(4-(diphenylamino)phenyl)thiophen-2-yl)thieno[3,4-b]pyrazin-5-yl)thiophene-2-carbaldehyde → 5-(7-(5-(4-(bis(4-(hexyloxy)phenyl)amino)phenyl)thiophen-2-yl)-2,3-bis(3,4-bis(hexyloxy)phenyl)thieno[3,4-b]pyrazin-5-yl)thiophene-2-carbaldehyde

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 100 ℃; Schlenk technique;

DOI:10.1039/c8ta04774j

upstream raw materials:

N,N-bis(4-hexyloxyphenyl)-4-bromophenylamine

tributyltin chloride

Downstream raw materials:

5-[N,N-bis(4-hexyloxyphenylamino)phenyl]-3,3'-diphenylsilylene-2,2'-bithiophene

C₄₇H₅₄BrNO₅S₂

C₄₄H₄₇NO₅S₃

C₃₈H₄₁NO₄S₃