C₄₅H₆₆O₅Si₂

Base Information

Chemical Name:C₄₅H₆₆O₅Si₂
CAS No.:1429412-70-3
Molecular Formula:C₄₅H₆₆O₅Si₂
Molecular Weight:743.187
Hs Code.:

C<sub>45</sub>H<sub>66</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₄₅H₆₆O₅Si₂

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Chemical Property of C₄₅H₆₆O₅Si₂

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Technology Process of C₄₅H₆₆O₅Si₂

There total 25 articles about C₄₅H₆₆O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1429412-53-2
C₁₃H₁₆O

: 1429412-68-9
C₄₂H₇₂O₄SSi₂

: 1429412-70-3
C₄₅H₆₆O₅Si₂

Guidance literature:: With copper(l) iodide; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; triethylamine; triphenylphosphine; In N,N-dimethyl-formamide; at 60 ℃; for 9h;
DOI:10.1039/c3ob27508f

Reference yield:

: 1429412-35-0
C₂₈H₃₈O₅Si

: 1429412-70-3
C₄₅H₆₆O₅Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: methanol; toluene / 1 h / 110 °C / Sealed tube

2.1: potassium carbonate / acetone / 5 h

3.1: hydrogen / isopropyl alcohol / 6 h / 20 °C

4.1: trimethylaluminum / toluene; dichloromethane / 0.58 h / 0 °C

4.2: 1.17 h / 0 °C

5.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / 0 °C

6.1: triethylamine; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; copper(l) iodide; triphenylphosphine / N,N-dimethyl-formamide / 9 h / 60 °C

With 2,6-dimethylpyridine; copper(l) iodide; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; hydrogen; trimethylaluminum; potassium carbonate; triethylamine; triphenylphosphine; In methanol; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol; acetone; toluene;
DOI:10.1039/c3ob27508f

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1429412-70-3
C₄₅H₆₆O₅Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydride / nujol; tetrahydrofuran / 16.5 h / 0 °C

1.2: 3.3 h / 0 °C

2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 6 h / Reflux

3.1: (R)-Tol-BINAP; tetrabutylammonium triphenyldifluorosilicate; copper(II) bis(trifluoromethanesulfonate) / tetrahydrofuran / 16 h / -78 °C

4.1: methanol; toluene / 1 h / 110 °C / Sealed tube

5.1: tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 18 h / -35 °C

6.1: zinc(II) chloride / tetrahydrofuran / 3 h / Molecular sieve; Reflux

7.1: silver(l) oxide / diethyl ether / 1 h / Molecular sieve; Reflux

8.1: trimethylaluminum / toluene; dichloromethane / 0.58 h / 0 °C

8.2: 1.17 h / 0 °C

9.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / 0 °C

10.1: triethylamine; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; copper(l) iodide; triphenylphosphine / N,N-dimethyl-formamide / 9 h / 60 °C

With 2,6-dimethylpyridine; copper(l) iodide; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; (R)-Tol-BINAP; trimethylaluminum; copper(II) bis(trifluoromethanesulfonate); sodium hydride; acetic acid; triethylamine; triphenylphosphine; tetrabutylammonium triphenyldifluorosilicate; zinc(II) chloride; silver(l) oxide; tetramethylammonium triacetoxyborohydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; nujol; diethyl ether; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; 3.1: |Mukaiyama Aldol Addition;
DOI:10.1039/c3ob27508f