N-(p-bromobenzoyl)-L-alanylglycylglycine methyl ester

Base Information

Chemical Name:N-(p-bromobenzoyl)-L-alanylglycylglycine methyl ester
CAS No.:1310053-86-1
Molecular Formula:C₁₅H₁₈BrN₃O₅
Molecular Weight:400.229
Hs Code.:

Synonyms:N-(p-bromobenzoyl)-L-alanylglycylglycine methyl ester

Suppliers and Price of N-(p-bromobenzoyl)-L-alanylglycylglycine methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(p-bromobenzoyl)-L-alanylglycylglycine methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(p-bromobenzoyl)-L-alanylglycylglycine methyl ester

There total 3 articles about N-(p-bromobenzoyl)-L-alanylglycylglycine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 167417-05-2
N-(p-bromobenzoyl)-L-alanine

: 13059-60-4
glycylglycine hydrochloride

: 1310053-86-1
N-(p-bromobenzoyl)-L-alanylglycylglycine methyl ester

Guidance literature:: glycylglycine hydrochloride; With triethylamine; In N,N-dimethyl-formamide; for 0.166667h;

N-(p-bromobenzoyl)-L-alanine; In N,N-dimethyl-formamide; for 0.166667h;

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; water; N,N-dimethyl-formamide; at -10 - 20 ℃;
DOI:10.1016/j.molstruc.2011.03.058

Reference yield:

: 586-75-4
4-chlorobenzoyl chloride

: 1310053-86-1
N-(p-bromobenzoyl)-L-alanylglycylglycine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / water / 7 h

2.1: triethylamine / N,N-dimethyl-formamide / 0.17 h

2.2: 0.17 h

2.3: -10 - 20 °C

With triethylamine; sodium hydroxide; In water; N,N-dimethyl-formamide;
DOI:10.1016/j.molstruc.2011.03.058

Reference yield:

: 586-76-5
4-Bromobenzoic acid

: 1310053-86-1
N-(p-bromobenzoyl)-L-alanylglycylglycine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride

2.1: sodium hydroxide / water / 7 h

3.1: triethylamine / N,N-dimethyl-formamide / 0.17 h

3.2: 0.17 h

3.3: -10 - 20 °C

With thionyl chloride; triethylamine; sodium hydroxide; In water; N,N-dimethyl-formamide;
DOI:10.1016/j.molstruc.2011.03.058