C₁₃H₇NO₃S

Base Information

Chemical Name:C₁₃H₇NO₃S
CAS No.:1391056-71-5
Molecular Formula:C₁₃H₇NO₃S
Molecular Weight:257.269
Hs Code.:

C<sub>13</sub>H<sub>7</sub>NO<sub>3</sub>S

Synonyms:C₁₃H₇NO₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₇NO₃S

Chemical Property:

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Technology Process of C₁₃H₇NO₃S

There total 3 articles about C₁₃H₇NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1391056-62-4
C₁₅H₁₃NO₃S

: 1391056-71-5
C₁₃H₇NO₃S

Guidance literature:: With ammonium cerium (IV) nitrate; water; In acetonitrile; at 25 ℃; for 1h;
DOI:10.1016/j.tetlet.2012.05.123

Reference yield:

: 67184-41-2,34967-19-6
2,5‐dimethoxybenzaldoxime

: 1391056-71-5
C₁₃H₇NO₃S

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hypochlorite; triethylamine / dichloromethane; water / 20 h / 0 - 25 °C / Inert atmosphere

2: ammonium cerium (IV) nitrate; water / acetonitrile / 1 h / 25 °C

With sodium hypochlorite; ammonium cerium (IV) nitrate; water; triethylamine; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.tetlet.2012.05.123

Reference yield:

: 93-02-7
2,5-dimethoxybenzaldehyde

: 1391056-71-5
C₁₃H₇NO₃S

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride; sodium acetate / methanol / 2 h / 25 °C

2: sodium hypochlorite; triethylamine / dichloromethane; water / 20 h / 0 - 25 °C / Inert atmosphere

3: ammonium cerium (IV) nitrate; water / acetonitrile / 1 h / 25 °C

With sodium hypochlorite; ammonium cerium (IV) nitrate; hydroxylamine hydrochloride; water; sodium acetate; triethylamine; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.tetlet.2012.05.123