C₁₉H₂₅NO₇

Base Information

Chemical Name:C₁₉H₂₅NO₇
CAS No.:850359-87-4
Molecular Formula:C₁₉H₂₅NO₇
Molecular Weight:379.41
Hs Code.:

C<sub>19</sub>H<sub>25</sub>NO<sub>7</sub>

Synonyms:C₁₉H₂₅NO₇

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Chemical Property of C₁₉H₂₅NO₇

Chemical Property:

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Technology Process of C₁₉H₂₅NO₇

There total 13 articles about C₁₉H₂₅NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 850359-86-3
C₂₂H₂₉NO₇

: 850359-87-4
C₁₉H₂₅NO₇

Guidance literature:: With acetic acid; at 20 ℃;
DOI:10.1055/s-2004-837223

Reference yield:

: 2847-00-9
1,2:5,6-di-O-isopropylidene-α-D-hexofuran-3-ulose

: 850359-87-4
C₁₉H₂₅NO₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: toluene / 100 °C

2.1: 99 percent / DIBALH / CH₂Cl₂ / -20 °C

3.1: DBU / CH₂Cl₂ / -78 °C

4.1: K₂CO₃ / xylene / Heating

5.1: O₃ / CH₂Cl₂ / -78 °C

5.2: 90 percent / Et₃N / CH₂Cl₂ / 0 °C

6.1: 95 percent / tetrahydrofuran / 0 °C

7.1: 96 percent / DMSO; Ac₂O / 20 °C

8.1: 70 percent / NaBH₄; CeCl₃*7H₂O / CH₂Cl₂; methanol / -10 °C

9.1: 99 percent / DBU / CH₂Cl₂ / 20 °C

10.1: 93 percent / NaH; TBAI / dimethylformamide / 20 °C

11.1: 85 percent / aq. AcOH / 20 °C

With sodium tetrahydroborate; cerium(III) chloride; acetic anhydride; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; potassium carbonate; ozone; acetic acid; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; xylene; 4.1: Overman rearrangement;
DOI:10.1055/s-2004-837223

Reference yield:

: 57466-98-5
(Z)-ethyl 2-((3aR,5S,6aR)-5-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethylfuro[2,3-d][1,3]dioxol-6(3aH,5H,6aH)-ylidene)acetate

: 850359-87-4
C₁₉H₂₅NO₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: 99 percent / DIBALH / CH₂Cl₂ / -20 °C

2.1: DBU / CH₂Cl₂ / -78 °C

3.1: K₂CO₃ / xylene / Heating

4.1: O₃ / CH₂Cl₂ / -78 °C

4.2: 90 percent / Et₃N / CH₂Cl₂ / 0 °C

5.1: 95 percent / tetrahydrofuran / 0 °C

6.1: 96 percent / DMSO; Ac₂O / 20 °C

7.1: 70 percent / NaBH₄; CeCl₃*7H₂O / CH₂Cl₂; methanol / -10 °C

8.1: 99 percent / DBU / CH₂Cl₂ / 20 °C

9.1: 93 percent / NaH; TBAI / dimethylformamide / 20 °C

10.1: 85 percent / aq. AcOH / 20 °C

With sodium tetrahydroborate; cerium(III) chloride; acetic anhydride; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; potassium carbonate; ozone; acetic acid; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; xylene; 3.1: Overman rearrangement;
DOI:10.1055/s-2004-837223