N¹,N³,N⁵-tris(3-aminophenyl)-N¹,N³,N⁵-trimethylbenzene-1,3,5-tricarboxamide

Base Information

• Chemical Name: N¹,N³,N⁵-tris(3-aminophenyl)-N¹,N³,N⁵-trimethylbenzene-1,3,5-tricarboxamide
• CAS No.: 940301-04-2
• Molecular Formula: C₃₀H₃₀N₆O₃
• Molecular Weight: 522.607
• Mol file: 940301-04-2.mol

Synonyms:N¹,N³,N⁵-tris(3-aminophenyl)-N¹,N³,N⁵-trimethylbenzene-1,3,5-tricarboxamide

Chemical Property of N¹,N³,N⁵-tris(3-aminophenyl)-N¹,N³,N⁵-trimethylbenzene-1,3,5-tricarboxamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N¹,N³,N⁵-tris(3-aminophenyl)-N¹,N³,N⁵-trimethylbenzene-1,3,5-tricarboxamide

There total 1 articles about N¹,N³,N⁵-tris(3-aminophenyl)-N¹,N³,N⁵-trimethylbenzene-1,3,5-tricarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

N1,N3,N5-Trimethyl-N1,N3,N5-tris(3-nitrophenyl)benzene-1,3,5-tricarboxamide (940301-03-1) → N1,N3,N5-tris(3-aminophenyl)-N1,N3,N5-trimethylbenzene-1,3,5-tricarboxamide (940301-04-2)

Guidance literature:

With palladium 10% on activated carbon; hydrazine hydrate; In ethanol; at 95 ℃; Microwave irradiation;

DOI:10.1016/j.chempr.2019.06.023

Reference yield: 79.0%

N1,N3,N5-tris(3-aminophenyl)-N1,N3,N5-trimethylbenzene-1,3,5-tricarboxamide (940301-04-2) + p-trifluoromethyl-phenylisocyanate (1548-13-6) → N1,N3,N5-trimethyl-N1,N3,N5-tris(3-(3-(4-(trifluoromethyl)phenyl)ureido)phenyl)benzene-1,3,5-tricarboxamide

Guidance literature:

In acetonitrile; Microwave irradiation; Heating;

DOI:10.1016/j.chempr.2019.06.023

Reference yield: 31.0%

N1,N3,N5-tris(3-aminophenyl)-N1,N3,N5-trimethylbenzene-1,3,5-tricarboxamide (940301-04-2) + 2,4-diflurophenylisocyanate (59025-55-7) → N1,N3,N5-tris(3-(3-(2,4-difluorophenyl)ureido)phenyl)-N1,N3,N5-trimethylbenzene-1,3,5-tricarboxamide

Guidance literature:

In acetonitrile; for 120h; Reflux;

DOI:10.1016/j.chempr.2019.06.023

upstream raw materials:

N¹,N³,N⁵-Trimethyl-N¹,N³,N⁵-tris(3-nitrophenyl)benzene-1,3,5-tricarboxamide