3'-[4-(4-n-butyloxybenzoyloxy)benzoyloxy]-4-(10-undecen-1-yloxy)benzoyloxybiphenyl

Base Information

Chemical Name:3'-[4-(4-n-butyloxybenzoyloxy)benzoyloxy]-4-(10-undecen-1-yloxy)benzoyloxybiphenyl
CAS No.:882053-60-3
Molecular Formula:C₄₈H₅₀O₈
Molecular Weight:754.92
Hs Code.:

Synonyms:3'-[4-(4-n-butyloxybenzoyloxy)benzoyloxy]-4-(10-undecen-1-yloxy)benzoyloxybiphenyl

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Chemical Property of 3'-[4-(4-n-butyloxybenzoyloxy)benzoyloxy]-4-(10-undecen-1-yloxy)benzoyloxybiphenyl

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Technology Process of 3'-[4-(4-n-butyloxybenzoyloxy)benzoyloxy]-4-(10-undecen-1-yloxy)benzoyloxybiphenyl

There total 5 articles about 3'-[4-(4-n-butyloxybenzoyloxy)benzoyloxy]-4-(10-undecen-1-yloxy)benzoyloxybiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 882053-58-9
3'-[4-(4-n-butyloxybenzoyloxy)benzoyloxy]biphenyl-4-ol

: 59100-95-7
4-(10-undecenyloxy)benzoic acid

: 882053-60-3
3'-[4-(4-n-butyloxybenzoyloxy)benzoyloxy]-4-(10-undecen-1-yloxy)benzoyloxybiphenyl

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/ja057685t

Reference yield:

: 882053-57-8
4'-benzyloxy-3-[4-(4-n-butyloxybenzoyloxy)benzoyloxy]biphenyl

: 882053-60-3
3'-[4-(4-n-butyloxybenzoyloxy)benzoyloxy]-4-(10-undecen-1-yloxy)benzoyloxybiphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / H₂ / Pd/C / tetrahydrofuran / 12 h / 40 °C / 2025.16 Torr

2: 70 percent / N,N'-dicyclohexylcarbodiimide; 4-N,N-dimethylaminopyridine / CH₂Cl₂ / 24 h / 20 °C

With dmap; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja057685t

Reference yield:

: 35065-86-2
3-bromophenyl acetate

: 882053-60-3
3'-[4-(4-n-butyloxybenzoyloxy)benzoyloxy]-4-(10-undecen-1-yloxy)benzoyloxybiphenyl

Guidance literature:: Multi-step reaction with 4 steps

1: 68 percent / Pd(PPh₃)4; aq. NaHCO₃ / 1,2-dimethoxy-ethane / 8 h / Heating

2: 70 percent / N,N'-dicyclohexylcarbodiimide; 4-N,N-dimethylaminopyridine / CH₂Cl₂ / 24 h / 20 °C

3: 74 percent / H₂ / Pd/C / tetrahydrofuran / 12 h / 40 °C / 2025.16 Torr

4: 70 percent / N,N'-dicyclohexylcarbodiimide; 4-N,N-dimethylaminopyridine / CH₂Cl₂ / 24 h / 20 °C

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane;
DOI:10.1021/ja057685t