benzyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Base Information

• Chemical Name: benzyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside
• CAS No.: 96323-23-8
• Molecular Formula: C₆₃H₆₆O₁₂
• Molecular Weight: 1015.21

Synonyms:benzyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Chemical Property of benzyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

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Technology Process of benzyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

There total 7 articles about benzyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

benzyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside (59935-49-8) + 2-O-acetyl-3,4,6-tri-O-benzyl-D-glucopyranose (79218-68-1,88988-46-9,93495-88-6,108869-76-7,127875-27-8,127875-34-7,129214-38-6,148968-88-1) → benzyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside (96323-23-8) + benzyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside (96323-23-8)

Guidance literature:

With silver trifluoromethanesulfonate; triethylamine; 4-Nitrobenzenesulfonyl chloride; In dichloromethane; at 0 ℃; for 24h;

DOI:10.1246/bcsj.58.120

Reference yield: 61.0%

benzyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside (59935-49-8) + 2-O-acetyl-3,4,6-tri-O-benzyl-D-glucopyranose (79218-68-1,88988-46-9,93495-88-6,108869-76-7,127875-27-8,127875-34-7,129214-38-6,148968-88-1) → benzyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside (96323-23-8) + benzyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside (96323-23-8)

Guidance literature:

With silver trifluoromethanesulfonate; triethylamine; 4-Nitrobenzenesulfonyl chloride; In dichloromethane; at 0 ℃; for 24h;

DOI:10.1246/bcsj.58.120

Reference yield: 41.0%

benzyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside (59935-49-8) + 2-O-acetyl-3,4,6-tri-O-benzyl-D-glucopyranose (79218-68-1,88988-46-9,93495-88-6,108869-76-7,127875-27-8,127875-34-7,129214-38-6,148968-88-1) → benzyl 6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-glucopyranoside (96323-23-8)

Guidance literature:

With methanesulfonic acid; cobalt(II) bromide; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1246/bcsj.58.120

upstream raw materials:

benzyl 2,3,4-tri-O-benzyl-α-D-glucopyranoside

2-O-acetyl-3,4,6-tri-O-benzyl-D-glucopyranose

benzyl chloride

β-D-glucose pentaacetate

Downstream raw materials:

benzyl 2,3,4-tri-O-benzyl-6-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-α-D-glucopyranoside

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