1-<3-methoxy-4-(3-methoxycarbonylphenoxy)phenyl>-2-<4-methoxy-3-(4-methoxycarbonylphenoxy)phenyl>ethane

Base Information

Chemical Name:1-<3-methoxy-4-(3-methoxycarbonylphenoxy)phenyl>-2-<4-methoxy-3-(4-methoxycarbonylphenoxy)phenyl>ethane
CAS No.:103561-04-2
Molecular Formula:C₃₂H₃₀O₈
Molecular Weight:542.585
Hs Code.:

Synonyms:1-<3-methoxy-4-(3-methoxycarbonylphenoxy)phenyl>-2-<4-methoxy-3-(4-methoxycarbonylphenoxy)phenyl>ethane

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Chemical Property of 1-<3-methoxy-4-(3-methoxycarbonylphenoxy)phenyl>-2-<4-methoxy-3-(4-methoxycarbonylphenoxy)phenyl>ethane

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Technology Process of 1-<3-methoxy-4-(3-methoxycarbonylphenoxy)phenyl>-2-<4-methoxy-3-(4-methoxycarbonylphenoxy)phenyl>ethane

There total 15 articles about 1-<3-methoxy-4-(3-methoxycarbonylphenoxy)phenyl>-2-<4-methoxy-3-(4-methoxycarbonylphenoxy)phenyl>ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 103561-03-1
C₃₂H₂₈O₉

: 103561-04-2
1-<3-methoxy-4-(3-methoxycarbonylphenoxy)phenyl>-2-<4-methoxy-3-(4-methoxycarbonylphenoxy)phenyl>ethane

Guidance literature:: With Clemensen reduction;
DOI:10.1016/S0040-4039(00)94949-9

Reference yield:

: 618-89-3
methyl 3-bromobenzoate

: 103561-04-2
1-<3-methoxy-4-(3-methoxycarbonylphenoxy)phenyl>-2-<4-methoxy-3-(4-methoxycarbonylphenoxy)phenyl>ethane

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) acid

2: 1.) NaBH₄, 2.) PBr₃ / 2.) pyridine

3: 50 percent / Zn, PdCl₂(PPh₃)2 / 1,2-dimethoxy-ethane / 20 h / Ambient temperature

4: 91 percent / Clemensen reduction

With bis-triphenylphosphine-palladium(II) chloride; sodium tetrahydroborate; phosphorus tribromide; zinc; In 1,2-dimethoxyethane;
DOI:10.1016/S0040-4039(00)94949-9

Reference yield:

: 619-42-1
4-methoxycarbonylphenyl bromide

: 103561-04-2
1-<3-methoxy-4-(3-methoxycarbonylphenoxy)phenyl>-2-<4-methoxy-3-(4-methoxycarbonylphenoxy)phenyl>ethane

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent

2: 1.) CrO₃, 2.) oxalyl chloride

3: 50 percent / Zn, PdCl₂(PPh₃)2 / 1,2-dimethoxy-ethane / 20 h / Ambient temperature

4: 91 percent / Clemensen reduction

With chromium(VI) oxide; bis-triphenylphosphine-palladium(II) chloride; oxalyl dichloride; zinc; In 1,2-dimethoxyethane;
DOI:10.1016/S0040-4039(00)94949-9