diethyl (2,3-O-isopropylidene-5-O-tert-butyldiphenylsilanyl-D-ribofuranos-1yl)difluoromethylenephosphonate

Base Information

Chemical Name:diethyl (2,3-O-isopropylidene-5-O-tert-butyldiphenylsilanyl-D-ribofuranos-1yl)difluoromethylenephosphonate
CAS No.:934817-79-5
Molecular Formula:C₂₉H₄₁F₂O₇PSi
Molecular Weight:598.696
Hs Code.:

Synonyms:diethyl (2,3-O-isopropylidene-5-O-tert-butyldiphenylsilanyl-D-ribofuranos-1yl)difluoromethylenephosphonate

Suppliers and Price of diethyl (2,3-O-isopropylidene-5-O-tert-butyldiphenylsilanyl-D-ribofuranos-1yl)difluoromethylenephosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of diethyl (2,3-O-isopropylidene-5-O-tert-butyldiphenylsilanyl-D-ribofuranos-1yl)difluoromethylenephosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of diethyl (2,3-O-isopropylidene-5-O-tert-butyldiphenylsilanyl-D-ribofuranos-1yl)difluoromethylenephosphonate

There total 1 articles about diethyl (2,3-O-isopropylidene-5-O-tert-butyldiphenylsilanyl-D-ribofuranos-1yl)difluoromethylenephosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 75-61-6
dibromodifluoromethane

: 5707-06-2
O,O-diethyl Se-phenyl phosphoroselenoate

: 130222-84-3
5-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-D-ribono-1,4-lactone

: 934817-79-5
diethyl (2,3-O-isopropylidene-5-O-tert-butyldiphenylsilanyl-D-ribofuranos-1yl)difluoromethylenephosphonate

Guidance literature:: dibromodifluoromethane; 5-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-D-ribono-1,4-lactone; In tetrahydrofuran; at -20 - 20 ℃; for 1h; vacuum;

With zinc; In tetrahydrofuran; for 15h; Heating / reflux;

O,O-diethyl Se-phenyl phosphoroselenoate; With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; more than 3 stages;