C₁₄H₂₀O₃

Base Information

Chemical Name:C₁₄H₂₀O₃
CAS No.:902131-81-1
Molecular Formula:C₁₄H₂₀O₃
Molecular Weight:236.311
Hs Code.:

C<sub>14</sub>H<sub>20</sub>O<sub>3</sub>

Synonyms:C₁₄H₂₀O₃

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Chemical Property of C₁₄H₂₀O₃

Chemical Property:

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Technology Process of C₁₄H₂₀O₃

There total 3 articles about C₁₄H₂₀O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 902131-80-0
C₁₄H₂₂O₃

: 902131-81-1
C₁₄H₂₀O₃

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 25 ℃; for 1h;
DOI:10.1039/b602020h

Reference yield:

: 902131-79-7
C₃₃H₃₆O₃

: 902131-81-1
C₁₄H₂₀O₃

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / TsOH*H₂O / methanol / 0.33 h / 25 °C

2: 99 percent / (COCl)2; Et₃N; DMSO / CH₂Cl₂ / 1 h / -78 - 25 °C

With oxalyl dichloride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; In methanol; dichloromethane; 2: Swern oxidation;
DOI:10.1039/b602020h

Reference yield:

: 902131-78-6
C₂₅H₂₈O₂

: 902131-81-1
C₁₄H₂₀O₃

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / NaH; tetra-n-butylammonium iodide / tetrahydrofuran / 36 h / 45 - 55 °C

2: 90 percent / TsOH*H₂O / methanol / 0.33 h / 25 °C

3: 99 percent / (COCl)2; Et₃N; DMSO / CH₂Cl₂ / 1 h / -78 - 25 °C

With oxalyl dichloride; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; 3: Swern oxidation;
DOI:10.1039/b602020h