6-(2-fluorophenyl)-[1,3]dioxolo[4,5-g]quinolin-8-yl 3,4,5-trimethoxybenzenesulfonate

Base Information

Chemical Name:6-(2-fluorophenyl)-[1,3]dioxolo[4,5-g]quinolin-8-yl 3,4,5-trimethoxybenzenesulfonate
CAS No.:1313356-74-9
Molecular Formula:C₂₅H₂₀FNO₈S
Molecular Weight:513.5
Hs Code.:

Synonyms:6-(2-fluorophenyl)-[1,3]dioxolo[4,5-g]quinolin-8-yl 3,4,5-trimethoxybenzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(2-fluorophenyl)-[1,3]dioxolo[4,5-g]quinolin-8-yl 3,4,5-trimethoxybenzenesulfonate

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Technology Process of 6-(2-fluorophenyl)-[1,3]dioxolo[4,5-g]quinolin-8-yl 3,4,5-trimethoxybenzenesulfonate

There total 2 articles about 6-(2-fluorophenyl)-[1,3]dioxolo[4,5-g]quinolin-8-yl 3,4,5-trimethoxybenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1313356-86-3,154554-41-3
CHM-2133

: 39614-62-5
3,4,5-trimethoxybenzenesulfonyl chloride

: 1313356-74-9
6-(2-fluorophenyl)-[1,3]dioxolo[4,5-g]quinolin-8-yl 3,4,5-trimethoxybenzenesulfonate

Guidance literature:: CHM-2133; With potassium carbonate; In N,N-dimethyl-formamide; for 0.333333h; Sonication;

3,4,5-trimethoxybenzenesulfonyl chloride; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1002/cmdc.201100121

Reference yield:

: 24313-88-0
3,4,5-Trimethoxyaniline

: 1313356-74-9
6-(2-fluorophenyl)-[1,3]dioxolo[4,5-g]quinolin-8-yl 3,4,5-trimethoxybenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; acetic acid; sodium nitrite / water; acetonitrile / 0.5 h / 0 °C

1.2: 2 h

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.33 h / Sonication

2.2: 0 - 20 °C

With hydrogenchloride; potassium carbonate; acetic acid; sodium nitrite; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cmdc.201100121