C₂₇H₄₆O₄Si

Base Information

Chemical Name:C₂₇H₄₆O₄Si
CAS No.:1268269-07-3
Molecular Formula:C₂₇H₄₆O₄Si
Molecular Weight:462.745
Hs Code.:

C<sub>27</sub>H<sub>46</sub>O<sub>4</sub>Si

Synonyms:C₂₇H₄₆O₄Si

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Chemical Property of C₂₇H₄₆O₄Si

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Technology Process of C₂₇H₄₆O₄Si

There total 9 articles about C₂₇H₄₆O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1268268-88-7
C₃₃H₆₀O₄Si₂

: 1268269-07-3
C₂₇H₄₆O₄Si

Guidance literature:: With camphor-10-sulfonic acid; In methanol; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja200089f

Reference yield:

: 1268268-84-3
C₂₄H₂₈O₄

: 1268269-07-3
C₂₇H₄₆O₄Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 3,3-dimethyldioxirane / dichloromethane / -78 - 0 °C / Inert atmosphere

1.2: 1.17 h / -78 - 0 °C / Inert atmosphere

1.3: 0 °C

2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

3.1: diethyl ether; toluene / 0.67 h / -78 - 0 °C / Inert atmosphere

4.1: dmap; triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

5.1: pyridinium p-toluenesulfonate / methanol / 3 h / 65 °C / Inert atmosphere

6.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

6.2: 0.5 h / -78 - 20 °C / Inert atmosphere

7.1: copper(l) iodide / tetrahydrofuran / 1 h / -78 - 0 °C / Inert atmosphere

7.2: 2 h / -40 °C / Inert atmosphere

8.1: camphor-10-sulfonic acid / methanol / 1 h / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; dmap; copper(l) iodide; tetrapropylammonium perruthennate; camphor-10-sulfonic acid; 3,3-dimethyldioxirane; pyridinium p-toluenesulfonate; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ja200089f

Reference yield:

: C₂₈H₃₆O₄

: 1268269-07-3
C₂₇H₄₆O₄Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride

2.1: 3,3-dimethyldioxirane / dichloromethane / -78 - 0 °C / Inert atmosphere

2.2: 1.17 h / -78 - 0 °C / Inert atmosphere

2.3: 0 °C

3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

4.1: diethyl ether; toluene / 0.67 h / -78 - 0 °C / Inert atmosphere

5.1: dmap; triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

6.1: pyridinium p-toluenesulfonate / methanol / 3 h / 65 °C / Inert atmosphere

7.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

7.2: 0.5 h / -78 - 20 °C / Inert atmosphere

8.1: copper(l) iodide / tetrahydrofuran / 1 h / -78 - 0 °C / Inert atmosphere

8.2: 2 h / -40 °C / Inert atmosphere

9.1: camphor-10-sulfonic acid / methanol / 1 h / 0 - 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,6-dimethylpyridine; dmap; copper(l) iodide; tetrapropylammonium perruthennate; camphor-10-sulfonic acid; 3,3-dimethyldioxirane; pyridinium p-toluenesulfonate; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ja200089f