4-{5-[2-(2-methoxy-ethoxy)-ethylamino]-1H-benzoimidazol-2-yl}-benzene-1,2-diamine

Base Information

Chemical Name:4-{5-[2-(2-methoxy-ethoxy)-ethylamino]-1H-benzoimidazol-2-yl}-benzene-1,2-diamine
CAS No.:1339046-88-6
Molecular Formula:C₁₈H₂₃N₅O₂
Molecular Weight:341.413
Hs Code.:

Synonyms:4-{5-[2-(2-methoxy-ethoxy)-ethylamino]-1H-benzoimidazol-2-yl}-benzene-1,2-diamine

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Chemical Property of 4-{5-[2-(2-methoxy-ethoxy)-ethylamino]-1H-benzoimidazol-2-yl}-benzene-1,2-diamine

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Technology Process of 4-{5-[2-(2-methoxy-ethoxy)-ethylamino]-1H-benzoimidazol-2-yl}-benzene-1,2-diamine

There total 4 articles about 4-{5-[2-(2-methoxy-ethoxy)-ethylamino]-1H-benzoimidazol-2-yl}-benzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1339046-85-3
[2-(4-amino-3-nitro-phenyl)-1H-benzoimidazol-5-yl]-[2-(2-methoxy-ethoxy)-ethyl]-amine

: 1339046-88-6
4-{5-[2-(2-methoxy-ethoxy)-ethylamino]-1H-benzoimidazol-2-yl}-benzene-1,2-diamine

Guidance literature:: With hydrogen; 5%-palladium/activated carbon; In methanol; ethyl acetate; at 20 ℃; for 24h; Inert atmosphere;

Reference yield:

: 1635-61-6
5-chloro-2-nitroaniline

: 1339046-88-6
4-{5-[2-(2-methoxy-ethoxy)-ethylamino]-1H-benzoimidazol-2-yl}-benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / ISOPROPYLAMIDE / 72 h / 120 °C / Inert atmosphere

2.1: hydrogen; acetic acid / 5%-palladium/activated carbon / ethanol / 24 h / 20 °C / Inert atmosphere

2.2: 17 h / 80 °C / Inert atmosphere

2.3: 4 °C

3.1: hydrogen / 5%-palladium/activated carbon / ethyl acetate; methanol / 24 h / 20 °C / Inert atmosphere

With hydrogen; potassium carbonate; acetic acid; 5%-palladium/activated carbon; In methanol; ethanol; ISOPROPYLAMIDE; ethyl acetate;

Reference yield:

: 31576-51-9,80506-64-5,869718-87-6
2-(2-methoxyethoxy)ethanamine

: 1339046-88-6
4-{5-[2-(2-methoxy-ethoxy)-ethylamino]-1H-benzoimidazol-2-yl}-benzene-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / ISOPROPYLAMIDE / 72 h / 120 °C / Inert atmosphere

2.1: hydrogen; acetic acid / 5%-palladium/activated carbon / ethanol / 24 h / 20 °C / Inert atmosphere

2.2: 17 h / 80 °C / Inert atmosphere

2.3: 4 °C

3.1: hydrogen / 5%-palladium/activated carbon / ethyl acetate; methanol / 24 h / 20 °C / Inert atmosphere

With hydrogen; potassium carbonate; acetic acid; 5%-palladium/activated carbon; In methanol; ethanol; ISOPROPYLAMIDE; ethyl acetate;