5-[(1E)-2-[4-(dioctylamino)phenyl]ethenyl]-2-furanecarboxaldehyde

Base Information

• Chemical Name: 5-[(1E)-2-[4-(dioctylamino)phenyl]ethenyl]-2-furanecarboxaldehyde
• CAS No.: 933037-96-8
• Molecular Formula: C₂₉H₄₃NO₂
• Molecular Weight: 437.666
• Mol file: 933037-96-8.mol

Synonyms:5-[(1E)-2-[4-(dioctylamino)phenyl]ethenyl]-2-furanecarboxaldehyde

Chemical Property of 5-[(1E)-2-[4-(dioctylamino)phenyl]ethenyl]-2-furanecarboxaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 5-[(1E)-2-[4-(dioctylamino)phenyl]ethenyl]-2-furanecarboxaldehyde

There total 4 articles about 5-[(1E)-2-[4-(dioctylamino)phenyl]ethenyl]-2-furanecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-[2-[4-(dioctylamino)phenyl]ethenyl]-2-furanecarboxaldehyde → 5-[(1E)-2-[4-(dioctylamino)phenyl]ethenyl]-2-furanecarboxaldehyde (933037-96-8)

Guidance literature:

With iodine; In dichloromethane; at 20 ℃; Irradiation;

DOI:10.1002/chem.200600689

Reference yield:

C31H47NO3 → 5-[(1E)-2-[4-(dioctylamino)phenyl]ethenyl]-2-furanecarboxaldehyde (933037-96-8)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl / tetrahydrofuran / 20 °C

2: 832 mg / iodine / CH₂Cl₂ / 20 °C / Irradiation

With hydrogenchloride; iodine; In tetrahydrofuran; dichloromethane;

DOI:10.1002/chem.200600689

Reference yield:

5-(1,3-dioxolan-2-yl)furan-2-carbaldehyde (117953-13-6) → 5-[(1E)-2-[4-(dioctylamino)phenyl]ethenyl]-2-furanecarboxaldehyde (933037-96-8)

Guidance literature:

Multi-step reaction with 3 steps

1: t-BuOK / CH₂Cl₂ / 20 °C

2: aq. HCl / tetrahydrofuran / 20 °C

3: 832 mg / iodine / CH₂Cl₂ / 20 °C / Irradiation

With hydrogenchloride; potassium tert-butylate; iodine; In tetrahydrofuran; dichloromethane; 1: Wittig condensation;

DOI:10.1002/chem.200600689

upstream raw materials:

5-(1,3-dioxolan-2-yl)furan-2-carbaldehyde