Technology Process of C24H36O8
There total 14 articles about C24H36O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen; acetic acid;
In
tetrahydrofuran;
for 4h;
Inert atmosphere;
DOI:10.1002/chem.201304776
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 20 °C / Inert atmosphere
2: palladium on activated charcoal; acetic acid; hydrogen / tetrahydrofuran / 4 h / Inert atmosphere
With
palladium on activated charcoal; hydrogen; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201304776
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylsilane; palladium 10% on activated carbon / dichloromethane / 16 h / Inert atmosphere
2.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.25 h / -78 °C / Inert atmosphere
2.2: 0.75 h / -78 °C / Inert atmosphere
3.1: diisobutylaluminium hydride / n-heptane; methanol; toluene / 1.75 h / -78 - 0 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C
5.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 20 °C / Inert atmosphere
6.1: palladium on activated charcoal; acetic acid; hydrogen / tetrahydrofuran / 4 h / Inert atmosphere
With
triethylsilane; palladium 10% on activated carbon; palladium on activated charcoal; tetrabutyl ammonium fluoride; hydrogen; tert.-butyl lithium; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid;
In
tetrahydrofuran; methanol; n-heptane; dichloromethane; toluene; pentane;
DOI:10.1002/chem.201304776