diprop-2-enyl N-<(4-<<4-(bis<2-chloroethyl>amino)phenoxycarbonyloxy>methyl>phenoxy)carbonyl>-L-glutamate

Base Information

Chemical Name:diprop-2-enyl N-<(4-<<4-(bis<2-chloroethyl>amino)phenoxycarbonyloxy>methyl>phenoxy)carbonyl>-L-glutamate
CAS No.:180839-00-3
Molecular Formula:C₃₀H₃₄Cl₂N₂O₉
Molecular Weight:637.514
Hs Code.:

Synonyms:diprop-2-enyl N-<(4-<<4-(bis<2-chloroethyl>amino)phenoxycarbonyloxy>methyl>phenoxy)carbonyl>-L-glutamate

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Chemical Property of diprop-2-enyl N-<(4-<<4-(bis<2-chloroethyl>amino)phenoxycarbonyloxy>methyl>phenoxy)carbonyl>-L-glutamate

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Technology Process of diprop-2-enyl N-<(4-<<4-(bis<2-chloroethyl>amino)phenoxycarbonyloxy>methyl>phenoxy)carbonyl>-L-glutamate

There total 8 articles about diprop-2-enyl N-<(4-<<4-(bis<2-chloroethyl>amino)phenoxycarbonyloxy>methyl>phenoxy)carbonyl>-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 180839-00-3
diprop-2-enyl N-<(4-<<4-(bis<2-chloroethyl>amino)phenoxycarbonyloxy>methyl>phenoxy)carbonyl>-L-glutamate

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / Et₃N / CHCl₃ / 2 h / Heating

2: 78 percent / sodium cyanoborohydride / acetic acid; methanol; H₂O / 1 h / Ambient temperature

3: 18-crown-6-ether, KF*HF / CH₂Cl₂ / 12 h

4: CH₂Cl₂ / 1 h

With potassium hydrogen bifluoride; 18-crown-6 ether; sodium cyanoborohydride; triethylamine; In methanol; dichloromethane; chloroform; water; acetic acid;
DOI:10.1021/jm980425k

Reference yield:

: 180839-12-7
diallyl L-glutamylisocyanate

: 180839-00-3
diprop-2-enyl N-<(4-<<4-(bis<2-chloroethyl>amino)phenoxycarbonyloxy>methyl>phenoxy)carbonyl>-L-glutamate

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / Et₃N / CHCl₃ / 2 h / Heating

2: 78 percent / sodium cyanoborohydride / acetic acid; methanol; H₂O / 1 h / Ambient temperature

3: 18-crown-6-ether, KF*HF / CH₂Cl₂ / 12 h

4: CH₂Cl₂ / 1 h

With potassium hydrogen bifluoride; 18-crown-6 ether; sodium cyanoborohydride; triethylamine; In methanol; dichloromethane; chloroform; water; acetic acid;
DOI:10.1021/jm980425k

Reference yield:

: 219591-98-7
diprop-2-enyl N-<(4-formylphenyloxy)carbonyl>-L-glutamate

: 180839-00-3
diprop-2-enyl N-<(4-<<4-(bis<2-chloroethyl>amino)phenoxycarbonyloxy>methyl>phenoxy)carbonyl>-L-glutamate

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / sodium cyanoborohydride / acetic acid; methanol; H₂O / 1 h / Ambient temperature

2: 18-crown-6-ether, KF*HF / CH₂Cl₂ / 12 h

3: CH₂Cl₂ / 1 h

With potassium hydrogen bifluoride; 18-crown-6 ether; sodium cyanoborohydride; In methanol; dichloromethane; water; acetic acid;
DOI:10.1021/jm980425k