Phosphoric acid 1-benzenesulfonyl-4-phenyl-1-(pyridin-2-ylsulfanyl)-butyl ester dimethyl ester

Base Information

Chemical Name:Phosphoric acid 1-benzenesulfonyl-4-phenyl-1-(pyridin-2-ylsulfanyl)-butyl ester dimethyl ester
CAS No.:135967-12-3
Molecular Formula:C₂₃H₂₆NO₆PS₂
Molecular Weight:507.568
Hs Code.:

Synonyms:Phosphoric acid 1-benzenesulfonyl-4-phenyl-1-(pyridin-2-ylsulfanyl)-butyl ester dimethyl ester

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Chemical Property of Phosphoric acid 1-benzenesulfonyl-4-phenyl-1-(pyridin-2-ylsulfanyl)-butyl ester dimethyl ester

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Technology Process of Phosphoric acid 1-benzenesulfonyl-4-phenyl-1-(pyridin-2-ylsulfanyl)-butyl ester dimethyl ester

There total 2 articles about Phosphoric acid 1-benzenesulfonyl-4-phenyl-1-(pyridin-2-ylsulfanyl)-butyl ester dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114050-31-6
3-Phenyl-propionic acid 2-thioxo-2H-pyridin-1-yl ester

: 135967-08-7
dimethyl 1-phenylsulfonylvinyl phosphate

: 135967-12-3
Phosphoric acid 1-benzenesulfonyl-4-phenyl-1-(pyridin-2-ylsulfanyl)-butyl ester dimethyl ester

Guidance literature:: In dichloromethane; at 0 - 5 ℃;
DOI:10.1016/S0040-4039(00)92693-5

Reference yield:

: 1121-30-8
1-hydroxy-2(1H)-pyridinethione

: 135967-12-3
Phosphoric acid 1-benzenesulfonyl-4-phenyl-1-(pyridin-2-ylsulfanyl)-butyl ester dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / DCC / CH₂Cl₂

2: 97 percent Spectr_. / CH₂Cl₂ / 0 - 5 °C

With dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/S0040-4039(00)92693-5