2-methoxy-6-propenyl-benzoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

Base Information

Chemical Name:2-methoxy-6-propenyl-benzoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester
CAS No.:438569-38-1
Molecular Formula:C₂₆H₃₄O₄
Molecular Weight:410.554
Hs Code.:

2-methoxy-6-propenyl-benzoic acid 2,6-di-<i>tert</i>-butyl-4-methoxy-phenyl ester

Synonyms:2-methoxy-6-propenyl-benzoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

Suppliers and Price of 2-methoxy-6-propenyl-benzoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-methoxy-6-propenyl-benzoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-methoxy-6-propenyl-benzoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

There total 1 articles about 2-methoxy-6-propenyl-benzoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 590-15-8
trans-2-propenyl bromide

: 215023-79-3
2,6-di-tert-butyl-4-methoxyphenyl 2,6-dimethoxybenzoic acid ester

: 438569-38-1
2-methoxy-6-propenyl-benzoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

Guidance literature:: trans-2-propenyl bromide; With magnesium; In tetrahydrofuran;

2,6-di-tert-butyl-4-methoxyphenyl 2,6-dimethoxybenzoic acid ester; In tetrahydrofuran; benzene; at 20 ℃; for 12h; Further stages.;
DOI:10.1039/b109396g

Reference yield: 81.0%

: 438569-38-1
2-methoxy-6-propenyl-benzoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

: 143112-20-3
2-methoxy-6-((E)-prop-1-enyl)benzoic acid

Guidance literature:: 2-methoxy-6-propenyl-benzoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester; With sodium methylate; In N,N,N,N,N,N-hexamethylphosphoric triamide; toluene; for 24h; Heating;

With water; In N,N,N,N,N,N-hexamethylphosphoric triamide; toluene; for 2h; Further stages.; Heating;
DOI:10.1039/b109396g

Reference yield:

: 438569-38-1
2-methoxy-6-propenyl-benzoic acid 2,6-di-tert-butyl-4-methoxy-phenyl ester

: 438569-42-7
2-methyl-7-(2,4,6-trimethyl-phenyl)-inden-1-one

Guidance literature:: Multi-step reaction with 6 steps

1.1: MeONa / toluene; hexamethylphosphoric acid triamide / 24 h / Heating

1.2: 81 percent / H₂O / toluene; hexamethylphosphoric acid triamide / 2 h / Heating

2.1: 97 percent / TFAA / benzene / 24 h / 20 °C

3.1: Mg / diethyl ether

3.2: benzene; diethyl ether / 24 h / Heating

4.1: NaOMe / toluene; hexamethylphosphoric acid triamide / 24 h / Heating

4.2: 6.69 g / H₂O / toluene; hexamethylphosphoric acid triamide / 2 h / Heating

5.1: SOCl₂; DMF / 2 h / Heating

6.1: SnCl₄ / benzene / 0.33 h / 0 °C

6.2: 5.27 g / Et₃N / benzene / 3 h / Heating

With thionyl chloride; sodium methylate; tin(IV) chloride; magnesium; N,N-dimethyl-formamide; trifluoroacetic anhydride; In N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; toluene; benzene;
DOI:10.1039/b109396g