Benzyl (1S,2S)-1-benzyl-2-hydroxy-3-[2-{(2S)-2-[(methoxycarbonyl)amino]-3,3-dimethylbutanoyl}-1-(4-nitrobenzyl)hydrazino]propylcarbamate

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Chemical Name:Benzyl (1S,2S)-1-benzyl-2-hydroxy-3-[2-{(2S)-2-[(methoxycarbonyl)amino]-3,3-dimethylbutanoyl}-1-(4-nitrobenzyl)hydrazino]propylcarbamate
CAS No.:857904-43-9
Molecular Formula:C₃₃H₄₁N₅O₈
Molecular Weight:635.717
Hs Code.:

Synonyms:Benzyl (1S,2S)-1-benzyl-2-hydroxy-3-[2-{(2S)-2-[(methoxycarbonyl)amino]-3,3-dimethylbutanoyl}-1-(4-nitrobenzyl)hydrazino]propylcarbamate

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Chemical Property of Benzyl (1S,2S)-1-benzyl-2-hydroxy-3-[2-{(2S)-2-[(methoxycarbonyl)amino]-3,3-dimethylbutanoyl}-1-(4-nitrobenzyl)hydrazino]propylcarbamate

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Technology Process of Benzyl (1S,2S)-1-benzyl-2-hydroxy-3-[2-{(2S)-2-[(methoxycarbonyl)amino]-3,3-dimethylbutanoyl}-1-(4-nitrobenzyl)hydrazino]propylcarbamate

There total 2 articles about Benzyl (1S,2S)-1-benzyl-2-hydroxy-3-[2-{(2S)-2-[(methoxycarbonyl)amino]-3,3-dimethylbutanoyl}-1-(4-nitrobenzyl)hydrazino]propylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 857904-42-8
Tert-butyl 2-((2S,3S)-3-{[(benzyloxy)carbonyl]amino}-2-hydroxy-4-phenylbutyl)-2-(4-nitrobenzyl)hydrazinecarboxylate

: 857904-43-9
Benzyl (1S,2S)-1-benzyl-2-hydroxy-3-[2-{(2S)-2-[(methoxycarbonyl)amino]-3,3-dimethylbutanoyl}-1-(4-nitrobenzyl)hydrazino]propylcarbamate

Guidance literature:: Tert-butyl 2-((2S,3S)-3-{[(benzyloxy)carbonyl]amino}-2-hydroxy-4-phenylbutyl)-2-(4-nitrobenzyl)hydrazinecarboxylate; With hydrogenchloride; water; In tetrahydrofuran; at 60 ℃; for 16h;

With triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; at 25 ℃; for 3h;

Reference yield: 86.0%

: 857904-43-9
Benzyl (1S,2S)-1-benzyl-2-hydroxy-3-[2-{(2S)-2-[(methoxycarbonyl)amino]-3,3-dimethylbutanoyl}-1-(4-nitrobenzyl)hydrazino]propylcarbamate

Guidance literature:

Reference yield: 27.0%

: 854754-25-9
C₁₅H₂₃N₃O₄S

: 857904-43-9
Benzyl (1S,2S)-1-benzyl-2-hydroxy-3-[2-{(2S)-2-[(methoxycarbonyl)amino]-3,3-dimethylbutanoyl}-1-(4-nitrobenzyl)hydrazino]propylcarbamate

: Methyl (1S)-1-{[2-((2S,3S)-2-hydroxy-3-{[(2S)-2-(3-{[2-(methoxymethyl)-1,3-thiazol-4-yl]methyl}-2-oxo-1-imidazolidinyl)-3,3-dimethylbutanoyl]amino}-4-phenylbutyl)hydrazino]carbonyl}-2,2-dimethylpropylcarbamate

Guidance literature:: Benzyl (1S,2S)-1-benzyl-2-hydroxy-3-[2-{(2S)-2-[(methoxycarbonyl)amino]-3,3-dimethylbutanoyl}-1-(4-nitrobenzyl)hydrazino]propylcarbamate; With hydrogen; palladium 10% on activated carbon; In methanol; at 25 ℃; for 2.5h;

C₁₅H₂₃N₃O₄S; With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In DMF (N,N-dimethyl-formamide); at 25 ℃; for 16h;