3-<α-hydrazino-α-(p-tolylamino)methyl>-4-hydroxy-6-methyl-2(1H)-quinolone

Base Information

Chemical Name:3-<α-hydrazino-α-(p-tolylamino)methyl>-4-hydroxy-6-methyl-2(1H)-quinolone
CAS No.:161152-13-2
Molecular Formula:C₁₈H₂₀N₄O₂
Molecular Weight:324.382
Hs Code.:

Synonyms:3-<α-hydrazino-α-(p-tolylamino)methyl>-4-hydroxy-6-methyl-2(1H)-quinolone

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Chemical Property of 3-<α-hydrazino-α-(p-tolylamino)methyl>-4-hydroxy-6-methyl-2(1H)-quinolone

Chemical Property:

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Technology Process of 3-<α-hydrazino-α-(p-tolylamino)methyl>-4-hydroxy-6-methyl-2(1H)-quinolone

There total 5 articles about 3-<α-hydrazino-α-(p-tolylamino)methyl>-4-hydroxy-6-methyl-2(1H)-quinolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 161152-11-0
3-<(p-tolylamino)bromomethyl>-4-hydroxy-6-methyl-2(1H)-quinolone

: 161152-13-2
3-<α-hydrazino-α-(p-tolylamino)methyl>-4-hydroxy-6-methyl-2(1H)-quinolone

Guidance literature:: With hydrazine hydrate; In ethanol; for 4h; Heating;

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 161152-13-2
3-<α-hydrazino-α-(p-tolylamino)methyl>-4-hydroxy-6-methyl-2(1H)-quinolone

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / ethane-1,2-diol / 100 - 190 °C

2: 79 percent / HBr / CHCl₃ / 2 h

3: 76 percent / hydrazine hydrate / ethanol / 4 h / Heating

With hydrogen bromide; hydrazine hydrate; In ethanol; chloroform; ethylene glycol;

Reference yield:

: 1677-44-7
4-hydroxy-6-methylquinolin-2(1H)-one

: 161152-13-2
3-<α-hydrazino-α-(p-tolylamino)methyl>-4-hydroxy-6-methyl-2(1H)-quinolone

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / ethane-1,2-diol / 100 - 190 °C

2: 79 percent / HBr / CHCl₃ / 2 h

3: 76 percent / hydrazine hydrate / ethanol / 4 h / Heating

With hydrogen bromide; hydrazine hydrate; In ethanol; chloroform; ethylene glycol;