5-(Bromomethyl)-6-chloro-2,1,3-benzothiadiazole

Base Information

Chemical Name:5-(Bromomethyl)-6-chloro-2,1,3-benzothiadiazole
CAS No.:65858-51-7
Molecular Formula:C₇H₄BrClN₂S
Molecular Weight:263.545
Hs Code.:2934999090
DSSTox Substance ID:DTXSID00381508
Wikidata:Q82172375
Mol file:65858-51-7.mol

Synonyms:65858-51-7;5-(bromomethyl)-6-chloro-2,1,3-benzothiadiazole;6-(bromomethyl)-5-chloro-2,1,3-benzothiadiazole;5-(Bromomethyl)-6-chlorobenzo[c][1,2,5]thiadiazole;SCHEMBL3392270;DTXSID00381508;FT-0619696;tert-Butyl(5-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-3-yl)methylcarbamate

Suppliers and Price of 5-(Bromomethyl)-6-chloro-2,1,3-benzothiadiazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5-(BROMOMETHYL)-6-CHLORO-2,1,3-BENZOTHIADIAZOLE 95.00%
1G
$ 881.67

Total 8 raw suppliers

Chemical Property of 5-(Bromomethyl)-6-chloro-2,1,3-benzothiadiazole

Chemical Property:

Vapor Pressure:0.000304mmHg at 25°C
Melting Point:75oC
Boiling Point:331.2oC at 760 mmHg
Flash Point:154.1oC
PSA：54.02000
Density:1.87g/cm3
LogP:3.23960
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:261.89671
Heavy Atom Count:12
Complexity:172

Purity/Quality:

98%Min ^*data from raw suppliers

5-(BROMOMETHYL)-6-CHLORO-2,1,3-BENZOTHIADIAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s): C
Hazard Codes: C:Corrosive;
Statements: R34:Causes burns.;
Safety Statements: S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.; S36/37/39:Wear suitabl

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C(=CC2=NSN=C21)Cl)CBr

Technology Process of 5-(Bromomethyl)-6-chloro-2,1,3-benzothiadiazole

There total 1 articles about 5-(Bromomethyl)-6-chloro-2,1,3-benzothiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50636-02-7
5-Chlor-6-methyl-2,1,3-benzothiadiazol

: 65858-51-7
5-bromomethyl-6-chloro-benzo[1,2,5]thiadiazole

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane;

Reference yield:

: 65858-51-7
5-bromomethyl-6-chloro-benzo[1,2,5]thiadiazole

: 1273317-50-2
C₁₆H₁₉ClN₆O₅S

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 12 h / 60 °C

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 24 h / 20 °C

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/jm101204u